5,6-dihydrocyclopentacenaphthylene-1,2-dione mono-p-toluenesulfonylhydrazone

Base Information

Chemical Name:5,6-dihydrocyclopentacenaphthylene-1,2-dione mono-p-toluenesulfonylhydrazone
CAS No.:98361-87-6
Molecular Formula:C₂₁H₁₆N₂O₃S
Molecular Weight:376.436
Hs Code.:

5,6-dihydrocyclopent<fg>acenaphthylene-1,2-dione mono-p-toluenesulfonylhydrazone

Synonyms:5,6-dihydrocyclopentacenaphthylene-1,2-dione mono-p-toluenesulfonylhydrazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5,6-dihydrocyclopentacenaphthylene-1,2-dione mono-p-toluenesulfonylhydrazone

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Technology Process of 5,6-dihydrocyclopentacenaphthylene-1,2-dione mono-p-toluenesulfonylhydrazone

There total 1 articles about 5,6-dihydrocyclopentacenaphthylene-1,2-dione mono-p-toluenesulfonylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 5254-01-3
1,2-diketopyracene

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 98361-87-6
5,6-dihydrocyclopentacenaphthylene-1,2-dione mono-p-toluenesulfonylhydrazone

Guidance literature:: In ethanol; for 24h; Heating;
DOI:10.1021/ja00311a063

Reference yield:

: 98361-87-6
5,6-dihydrocyclopentacenaphthylene-1,2-dione mono-p-toluenesulfonylhydrazone

: 5699-00-3
1,2-dihydro-6-oxacyclopentaphenalene-5,7-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / 0.1 N aq. sodium hydroxide / CH₂Cl₂ / 5 h / Ambient temperature

2: 18.33 h / Irradiation

With sodium hydroxide; In dichloromethane;
DOI:10.1021/ja00311a063