1-tert-butyl 3-ethyl 4-(1-phenylethylamino)piperidine-1,3-dicarboxylate

Base Information

Chemical Name:1-tert-butyl 3-ethyl 4-(1-phenylethylamino)piperidine-1,3-dicarboxylate
CAS No.:1058737-53-3
Molecular Formula:C₂₁H₃₂N₂O₄
Molecular Weight:376.496
Hs Code.:

Synonyms:1-tert-butyl 3-ethyl 4-(1-phenylethylamino)piperidine-1,3-dicarboxylate

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Chemical Property of 1-tert-butyl 3-ethyl 4-(1-phenylethylamino)piperidine-1,3-dicarboxylate

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Technology Process of 1-tert-butyl 3-ethyl 4-(1-phenylethylamino)piperidine-1,3-dicarboxylate

There total 3 articles about 1-tert-butyl 3-ethyl 4-(1-phenylethylamino)piperidine-1,3-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1058737-52-2
1-tert-butyl 3-ethyl 4-(1-phenylethylamino)-5,6-dihydropyridine-1,3(2H)-dicarboxylate

: 1058737-53-3
1-tert-butyl 3-ethyl 4-(1-phenylethylamino)piperidine-1,3-dicarboxylate

Guidance literature:: 1-tert-butyl 3-ethyl 4-(1-phenylethylamino)-5,6-dihydropyridine-1,3(2H)-dicarboxylate; With sodium tris(acetoxy)borohydride; acetic acid; In toluene; at -5 - 20 ℃; for 16h;

With water; sodium carbonate; pH=9;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1058737-53-3
1-tert-butyl 3-ethyl 4-(1-phenylethylamino)piperidine-1,3-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen; triethylamine / palladium(II) hydroxide/carbon / ethanol / 5 h / 3102.97 Torr

2.1: toluene / 16 h / Heating / reflux

3.1: sodium tris(acetoxy)borohydride; acetic acid / toluene / 16 h / -5 - 20 °C

3.2: pH 9

With hydrogen; sodium tris(acetoxy)borohydride; acetic acid; triethylamine; palladium(II) hydroxide/carbon; In ethanol; toluene;

Reference yield:

: 52763-21-0
ethyl 1-benzyl-3-oxopiperidine-4-carboxylate hydrochloride

: 1058737-53-3
1-tert-butyl 3-ethyl 4-(1-phenylethylamino)piperidine-1,3-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen; triethylamine / palladium(II) hydroxide/carbon / ethanol / 5 h / 3102.97 Torr

2.1: toluene / 16 h / Heating / reflux

3.1: sodium tris(acetoxy)borohydride; acetic acid / toluene / 16 h / -5 - 20 °C

3.2: pH 9

With hydrogen; sodium tris(acetoxy)borohydride; acetic acid; triethylamine; palladium(II) hydroxide/carbon; In ethanol; toluene;