bis{2-[m-(2-hydroxyethylthiaisopropyl)α,α-dimethylbenzylcarbamoyl]ethyl} terephthalate

Base Information

Chemical Name:bis{2-[m-(2-hydroxyethylthiaisopropyl)α,α-dimethylbenzylcarbamoyl]ethyl} terephthalate
CAS No.:1356927-83-7
Molecular Formula:C₄₂H₅₆N₂O₁₀S₂
Molecular Weight:813.046
Hs Code.:

Synonyms:bis{2-[m-(2-hydroxyethylthiaisopropyl)α,α-dimethylbenzylcarbamoyl]ethyl} terephthalate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis{2-[m-(2-hydroxyethylthiaisopropyl)α,α-dimethylbenzylcarbamoyl]ethyl} terephthalate

Chemical Property:

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Technology Process of bis{2-[m-(2-hydroxyethylthiaisopropyl)α,α-dimethylbenzylcarbamoyl]ethyl} terephthalate

There total 3 articles about bis{2-[m-(2-hydroxyethylthiaisopropyl)α,α-dimethylbenzylcarbamoyl]ethyl} terephthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1356927-80-4
C₃₈H₄₄N₂O₈

: 60-24-2
2-hydroxyethanethiol

: 1356927-83-7
bis{2-[m-(2-hydroxyethylthiaisopropyl)α,α-dimethylbenzylcarbamoyl]ethyl} terephthalate

Guidance literature:: With 2,2'-azobis(isobutyronitrile); In acetonitrile; at 75 ℃; for 4h; Inert atmosphere;
DOI:10.1080/10426507.2011.625512

Reference yield:

: 120-61-6
1,4-benzenedicarboxylic acid dimethyl ester

: 1356927-83-7
bis{2-[m-(2-hydroxyethylthiaisopropyl)α,α-dimethylbenzylcarbamoyl]ethyl} terephthalate

Guidance literature:: Multi-step reaction with 3 steps

1: zinc diacetate; chloroacetic acid / 24 h / 70 °C

2: dibutyltin dilaurate / tetrahydrofuran / 5 h / 80 °C / Inert atmosphere

3: 2,2'-azobis(isobutyronitrile) / acetonitrile / 4 h / 75 °C / Inert atmosphere

With 2,2'-azobis(isobutyronitrile); zinc diacetate; dibutyltin dilaurate; chloroacetic acid; In tetrahydrofuran; acetonitrile;
DOI:10.1080/10426507.2011.625512

Reference yield:

: 959-26-2
Bis(2-Hydroxyethyl)terephthalat

: 2094-99-7
1-(1-isocyanato-1-methylethyl)-3-(1-methylethenyl)benzene

: 1356927-83-7
bis{2-[m-(2-hydroxyethylthiaisopropyl)α,α-dimethylbenzylcarbamoyl]ethyl} terephthalate

Guidance literature:: Multi-step reaction with 2 steps

1: dibutyltin dilaurate / tetrahydrofuran / 5 h / 80 °C / Inert atmosphere

2: 2,2'-azobis(isobutyronitrile) / acetonitrile / 4 h / 75 °C / Inert atmosphere

With 2,2'-azobis(isobutyronitrile); dibutyltin dilaurate; In tetrahydrofuran; acetonitrile;
DOI:10.1080/10426507.2011.625512