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Technology Process of C5H5(C4H3(C6H5)3)ZrCl2(1-)*Li((CH3)2NCH2CH2N(CH3)2)2(1+)=[C5H5(C4H3(C6H5)3)ZrCl2][Li((CH3)2NCH2CH2N(CH3)2)2]

C5H5(C4H3(C6H5)3)ZrCl2(1-)*Li((CH3)2NCH2CH2N(CH3)2)2(1+)=[C5H5(C4H3(C6H5)3)ZrCl2][Li((CH3)2NCH2CH2N(CH3)2)2]

Base Information
  • Chemical Name:C5H5(C4H3(C6H5)3)ZrCl2(1-)*Li((CH3)2NCH2CH2N(CH3)2)2(1+)=[C5H5(C4H3(C6H5)3)ZrCl2][Li((CH3)2NCH2CH2N(CH3)2)2]
  • CAS No.:185856-55-7
  • Molecular Formula:C12H32LiN4*C27H23Cl2Zr
  • Molecular Weight:748.964
  • Hs Code.:
C<sub>5</sub>H<sub>5</sub>(C<sub>4</sub>H<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>)3)ZrCl<sub>2</sub><sup>(1-)</sup>*Li((CH<sub>3</sub>)2NCH<sub>2</sub>CH<sub>2</sub>N(CH<sub>3</sub>)2)2<sup>(1+)</sup>=[C<sub>5</sub>H<sub>5</sub>(C<sub>4</sub>H<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>)3)ZrCl<sub>2</sub>][Li((CH<sub>3</sub>)2NCH<sub>2</sub>CH<sub>2</sub>N(CH<sub>3</sub>)2)2]

Synonyms:C5H5(C4H3(C6H5)3)ZrCl2(1-)*Li((CH3)2NCH2CH2N(CH3)2)2(1+)=[C5H5(C4H3(C6H5)3)ZrCl2][Li((CH3)2NCH2CH2N(CH3)2)2]

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Chemical Property of C5H5(C4H3(C6H5)3)ZrCl2(1-)*Li((CH3)2NCH2CH2N(CH3)2)2(1+)=[C5H5(C4H3(C6H5)3)ZrCl2][Li((CH3)2NCH2CH2N(CH3)2)2]
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Technology Process of C5H5(C4H3(C6H5)3)ZrCl2(1-)*Li((CH3)2NCH2CH2N(CH3)2)2(1+)=[C5H5(C4H3(C6H5)3)ZrCl2][Li((CH3)2NCH2CH2N(CH3)2)2]

There total 1 articles about C5H5(C4H3(C6H5)3)ZrCl2(1-)*Li((CH3)2NCH2CH2N(CH3)2)2(1+)=[C5H5(C4H3(C6H5)3)ZrCl2][Li((CH3)2NCH2CH2N(CH3)2)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

(η5-cyclopentadienyl)trichlorozirconium dimethoxyethane

(η5-cyclopentadienyl)trichlorozirconium dimethoxyethane

Li<sup>(1+)</sup>*C<sub>4</sub>H<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>)3<sup>(2-)</sup>*Li((CH<sub>3</sub>)2NCH<sub>2</sub>CH<sub>2</sub>N(CH<sub>3</sub>)2)2<sup>(1+)</sup>=Li<sub>2</sub>(C<sub>4</sub>H<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>)3)((CH<sub>3</sub>)2NCH<sub>2</sub>CH<sub>2</sub>N(CH<sub>3</sub>)2)2
92314-26-6

Li(1+)*C4H3(C6H5)3(2-)*Li((CH3)2NCH2CH2N(CH3)2)2(1+)=Li2(C4H3(C6H5)3)((CH3)2NCH2CH2N(CH3)2)2

C<sub>5</sub>H<sub>5</sub>(C<sub>4</sub>H<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>)3)ZrCl<sub>2</sub><sup>(1-)</sup>*Li((CH<sub>3</sub>)2NCH<sub>2</sub>CH<sub>2</sub>N(CH<sub>3</sub>)2)2<sup>(1+)</sup>=[C<sub>5</sub>H<sub>5</sub>(C<sub>4</sub>H<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>)3)ZrCl<sub>2</sub>][Li((CH<sub>3</sub>)2NCH<sub>2</sub>CH<sub>2</sub>N(CH<sub>3</sub>)2)2]
185856-55-7

C5H5(C4H3(C6H5)3)ZrCl2(1-)*Li((CH3)2NCH2CH2N(CH3)2)2(1+)=[C5H5(C4H3(C6H5)3)ZrCl2][Li((CH3)2NCH2CH2N(CH3)2)2]

Guidance literature:
In toluene; stirring (3 h); evapn., heating (60°C, 1 h), extracting (dimethyl ether/benzene, 1/1), washing (pentane); elem. anal.;
DOI:10.1021/ja962545s
upstream raw materials:

Li(1+)*C4H3(C6H5)3(2-)*Li((CH3)2NCH2CH2N(CH3)2)2(1+)=Li2(C4H3(C6H5)3)((CH3)2NCH2CH2N(CH3)2)2

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