Technology Process of C28H21NO5
There total 3 articles about C28H21NO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
2: palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 20.5 h / 20 - 100 °C / Inert atmosphere; Schlenk technique
3: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
With
palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; trifluoroacetic acid;
In
dichloromethane; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 20.5 h / 20 - 100 °C / Inert atmosphere; Schlenk technique
2: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
With
palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; trifluoroacetic acid;
In
dichloromethane; toluene;