C₂₅H₃₂Cl₃NO₈

Base Information

Chemical Name:C₂₅H₃₂Cl₃NO₈
CAS No.:1262848-19-0
Molecular Formula:C₂₅H₃₂Cl₃NO₈
Molecular Weight:580.89
Hs Code.:

C<sub>25</sub>H<sub>32</sub>Cl<sub>3</sub>NO<sub>8</sub>

Synonyms:C₂₅H₃₂Cl₃NO₈

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Chemical Property of C₂₅H₃₂Cl₃NO₈

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Technology Process of C₂₅H₃₂Cl₃NO₈

There total 4 articles about C₂₅H₃₂Cl₃NO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1262848-17-8
C₂₅H₃₀Cl₃NO₆

: C₂₅H₃₂Cl₃NO₈

: 1262848-19-0
C₂₅H₃₂Cl₃NO₈

Guidance literature:: With methanesulfonamide; (9S,9"S)-9,9"-[phthalazine-1,4-diylbis-(oxy)]bis[10,11-dihydro-6'-methoxycinchonane]; In water; tert-butyl alcohol; at 0 ℃; for 62h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol102856j

Reference yield:

: C₂₃H₂₆Cl₃NO₅

: C₂₅H₃₂Cl₃NO₈

: 1262848-19-0
C₂₅H₃₂Cl₃NO₈

Guidance literature:: Multi-step reaction with 3 steps

1: 2,6-di-tert-butyl-4-methyl-phenol / tert-butylbenzene / 27 h / 180 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine; sodium iodide / 1,2-dichloro-ethane / 3 h / 40 °C / Inert atmosphere

3: methanesulfonamide; (9S,9"S)-9,9"-[phthalazine-1,4-diylbis-(oxy)]bis[10,11-dihydro-6'-methoxycinchonane] / water; tert-butyl alcohol / 62 h / 0 °C / Inert atmosphere

With methanesulfonamide; 2,6-di-tert-butyl-4-methyl-phenol; (9S,9"S)-9,9"-[phthalazine-1,4-diylbis-(oxy)]bis[10,11-dihydro-6'-methoxycinchonane]; N-ethyl-N,N-diisopropylamine; sodium iodide; In tert-butylbenzene; water; 1,2-dichloro-ethane; tert-butyl alcohol; 1: Overman rearrangement / 3: Sharpless dihydroxylation;
DOI:10.1021/ol102856j

Reference yield:

: 160836-05-5
C₂₁H₂₆O₅

: C₂₅H₃₂Cl₃NO₈

: 1262848-19-0
C₂₅H₃₂Cl₃NO₈

Guidance literature:: Multi-step reaction with 4 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 4 h / -5 - 0 °C / Inert atmosphere

2: 2,6-di-tert-butyl-4-methyl-phenol / tert-butylbenzene / 27 h / 180 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine; sodium iodide / 1,2-dichloro-ethane / 3 h / 40 °C / Inert atmosphere

4: methanesulfonamide; (9S,9"S)-9,9"-[phthalazine-1,4-diylbis-(oxy)]bis[10,11-dihydro-6'-methoxycinchonane] / water; tert-butyl alcohol / 62 h / 0 °C / Inert atmosphere

With methanesulfonamide; 2,6-di-tert-butyl-4-methyl-phenol; 1,8-diazabicyclo[5.4.0]undec-7-ene; (9S,9"S)-9,9"-[phthalazine-1,4-diylbis-(oxy)]bis[10,11-dihydro-6'-methoxycinchonane]; N-ethyl-N,N-diisopropylamine; sodium iodide; In tert-butylbenzene; dichloromethane; water; 1,2-dichloro-ethane; tert-butyl alcohol; 2: Overman rearrangement / 4: Sharpless dihydroxylation;
DOI:10.1021/ol102856j