C₂₂H₂₄O₄

Base Information

• Chemical Name: C₂₂H₂₄O₄
• CAS No.: 943860-42-2
• Molecular Formula: C₂₂H₂₄O₄
• Molecular Weight: 352.43
• Mol file: 943860-42-2.mol

Synonyms:C₂₂H₂₄O₄

Chemical Property of C₂₂H₂₄O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₂₄O₄

There total 5 articles about C₂₂H₂₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

1-(2-hydroxy-4-methoxyphenyl)ethanone (552-41-0) + 4-Methoxy-3-(γ,γ-dimethylallyl)benzaldehyde (56074-98-7) → C22H24O4 (943860-42-2)

Guidance literature:

With potassium hydroxide; at 20 ℃;

DOI:10.1021/jm070109i

Reference yield:

2-bromo-4-(1,3-dioxolan-2-yl)phenol (162271-15-0) → C22H24O4 (943860-42-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 91 percent / K₂CO₃ / acetone / 20 °C

2: 75 percent / aq. KOH / 20 °C

With potassium hydroxide; potassium carbonate; In acetone; 3: Claisen-Schmidt reaction;

DOI:10.1021/jm070109i

Reference yield:

2',4'-dihydroxy-4-acetophenone (89-84-9) → C22H24O4 (943860-42-2)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / acetone / 20 °C

2: 75 percent / aq. KOH / 20 °C

With potassium hydroxide; potassium carbonate; In acetone; 2: Claisen-Schmidt reaction;

DOI:10.1021/jm070109i

upstream raw materials:

1-(2-hydroxy-4-methoxyphenyl)ethanone

4-Methoxy-3-(γ,γ-dimethylallyl)benzaldehyde

2-bromo-4-(1,3-dioxolan-2-yl)phenol

2',4'-dihydroxy-4-acetophenone

Refernces