N-<1-(Methoxycarbonyl)propyl>-α-methoxy-α-<(trifluoromethyl)phenyl>acetamide

Base Information

Chemical Name:N-<1-(Methoxycarbonyl)propyl>-α-methoxy-α-<(trifluoromethyl)phenyl>acetamide
CAS No.:70363-18-7
Molecular Formula:C₁₅H₁₈F₃NO₄
Molecular Weight:333.307
Hs Code.:

Synonyms:N-<1-(Methoxycarbonyl)propyl>-α-methoxy-α-<(trifluoromethyl)phenyl>acetamide

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Chemical Property of N-<1-(Methoxycarbonyl)propyl>-α-methoxy-α-<(trifluoromethyl)phenyl>acetamide

Chemical Property:

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Technology Process of N-<1-(Methoxycarbonyl)propyl>-α-methoxy-α-<(trifluoromethyl)phenyl>acetamide

There total 6 articles about N-<1-(Methoxycarbonyl)propyl>-α-methoxy-α-<(trifluoromethyl)phenyl>acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56762-93-7
methyl (S)-2-(benzyloxycarbonylamino)-4-methylmercaptobutanoate

: 70363-18-7
N-<1-(Methoxycarbonyl)propyl>-α-methoxy-α-<(trifluoromethyl)phenyl>acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / NaIO₄ / H₂O; methanol / 3 h / 0 °C

2: 80 percent Chromat_. / 180 °C / var. temp. and pressures

3: 81 percent / H₂ / 5percent Pd/BaSO₄ / methanol / 0.75 h

4: N(C₂H₅)3 / CCl₄ / 2 h / 20 °C

With sodium periodate; hydrogen; triethylamine; Pd-BaSO₄; In methanol; tetrachloromethane; water;
DOI:10.1021/jo01312a002

Reference yield:

: 75266-39-6
methyl (S)-2-<<(benzyloxy)carbonyl>amino>-4-(methylsulfinyl)butanoate

: 70363-18-7
N-<1-(Methoxycarbonyl)propyl>-α-methoxy-α-<(trifluoromethyl)phenyl>acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent Chromat_. / 180 °C / var. temp. and pressures

2: 81 percent / H₂ / 5percent Pd/BaSO₄ / methanol / 0.75 h

3: N(C₂H₅)3 / CCl₄ / 2 h / 20 °C

With hydrogen; triethylamine; Pd-BaSO₄; In methanol; tetrachloromethane;
DOI:10.1021/jo01312a002

Reference yield:

: 2491-18-1
(S)-methyl 2-amino-4-(methylthio)butanoate hydrochloride

: 70363-18-7
N-<1-(Methoxycarbonyl)propyl>-α-methoxy-α-<(trifluoromethyl)phenyl>acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / KHCO₃ / H₂O; ethyl acetate / 4 h / 0 °C

2: 95 percent / NaIO₄ / H₂O; methanol / 3 h / 0 °C

3: 80 percent Chromat_. / 180 °C / var. temp. and pressures

4: 81 percent / H₂ / 5percent Pd/BaSO₄ / methanol / 0.75 h

5: N(C₂H₅)3 / CCl₄ / 2 h / 20 °C

With sodium periodate; hydrogen; potassium hydrogencarbonate; triethylamine; Pd-BaSO₄; In methanol; tetrachloromethane; water; ethyl acetate;
DOI:10.1021/jo01312a002