2-<<2-phenyl>amino>-4-amino-6-chloro-1,3,5-triazine

Base Information

Chemical Name:2-<<2-phenyl>amino>-4-amino-6-chloro-1,3,5-triazine
CAS No.:146651-76-5
Molecular Formula:C₁₄H₁₇ClN₆O₂
Molecular Weight:336.781
Hs Code.:

2-<<2-<N-(tert-butyloxycarbonyl)amino>phenyl>amino>-4-amino-6-chloro-1,3,5-triazine

Synonyms:2-<<2-phenyl>amino>-4-amino-6-chloro-1,3,5-triazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-<<2-phenyl>amino>-4-amino-6-chloro-1,3,5-triazine

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Technology Process of 2-<<2-phenyl>amino>-4-amino-6-chloro-1,3,5-triazine

There total 4 articles about 2-<<2-phenyl>amino>-4-amino-6-chloro-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [2-(4,6-Dichloro-[1,3,5]triazin-2-ylamino)-phenyl]-carbamic acid tert-butyl ester

: 146651-76-5
2-<<2-phenyl>amino>-4-amino-6-chloro-1,3,5-triazine

Guidance literature:: With ammonia; In tetrahydrofuran; for 1.5h; Yield given;
DOI:10.1021/ja00057a015

Reference yield:

: 58632-95-4
2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile

: 146651-76-5
2-<<2-phenyl>amino>-4-amino-6-chloro-1,3,5-triazine

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / Et₃N / dimethylformamide / 3 h / 55 °C

2: N,N-diisopropylethylamine (DIPEA) / tetrahydrofuran / 0.67 h

3: NH₃ (gas) / tetrahydrofuran / 1.5 h

With ammonia; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ja00057a015

Reference yield:

: 146651-75-4
tert–butyl (2–aminophenyl)carbamate

: 146651-76-5
2-<<2-phenyl>amino>-4-amino-6-chloro-1,3,5-triazine

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-diisopropylethylamine (DIPEA) / tetrahydrofuran / 0.67 h

2: NH₃ (gas) / tetrahydrofuran / 1.5 h

With ammonia; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;
DOI:10.1021/ja00057a015