Technology Process of C28H31N6O10P
There total 4 articles about C28H31N6O10P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C43H46ClN6O13P;
With
pyridine; tetrabutyl ammonium fluoride;
In
water;
at 40 ℃;
pH=7;
With
ammonium hydroxide;
In
water;
at 20 ℃;
for 48h;
DOI:10.3762/bjoc.9.326
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: pyridine; 1-methyl-1H-imidazole; 2,4,6-triisopropylphenylsulfonyl chloride
2.1: pyridine; tetrabutyl ammonium fluoride / water / 40 °C / pH 7
2.2: 48 h / 20 °C
With
pyridine; 1-methyl-1H-imidazole; 2,4,6-triisopropylphenylsulfonyl chloride; tetrabutyl ammonium fluoride;
In
water;
DOI:10.3762/bjoc.9.326
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: ammonium bicarbonate / 1,4-dioxane / 2 h
1.2: 2 h
2.1: pyridine; 1-methyl-1H-imidazole; 2,4,6-triisopropylphenylsulfonyl chloride
3.1: pyridine; tetrabutyl ammonium fluoride / water / 40 °C / pH 7
3.2: 48 h / 20 °C
With
pyridine; 1-methyl-1H-imidazole; 2,4,6-triisopropylphenylsulfonyl chloride; tetrabutyl ammonium fluoride; ammonium bicarbonate;
In
1,4-dioxane; water;
DOI:10.3762/bjoc.9.326