(3S,5S)-1-((S)-4-benzyl-2-thioxothiazolidin-3-yl)-5-(tert-butyldimethylsilyloxy)-7-(4-(tert-butyldimethylsilyloxy)phenyl)-3-hydroxyheptan-1-one

Base Information

• Chemical Name: (3S,5S)-1-((S)-4-benzyl-2-thioxothiazolidin-3-yl)-5-(tert-butyldimethylsilyloxy)-7-(4-(tert-butyldimethylsilyloxy)phenyl)-3-hydroxyheptan-1-one
• CAS No.: 1068608-46-7
• Molecular Formula: C₃₅H₅₅NO₄S₂Si₂
• Molecular Weight: 674.129

Synonyms:(3S,5S)-1-((S)-4-benzyl-2-thioxothiazolidin-3-yl)-5-(tert-butyldimethylsilyloxy)-7-(4-(tert-butyldimethylsilyloxy)phenyl)-3-hydroxyheptan-1-one

Chemical Property of (3S,5S)-1-((S)-4-benzyl-2-thioxothiazolidin-3-yl)-5-(tert-butyldimethylsilyloxy)-7-(4-(tert-butyldimethylsilyloxy)phenyl)-3-hydroxyheptan-1-one

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Technology Process of (3S,5S)-1-((S)-4-benzyl-2-thioxothiazolidin-3-yl)-5-(tert-butyldimethylsilyloxy)-7-(4-(tert-butyldimethylsilyloxy)phenyl)-3-hydroxyheptan-1-one

There total 1 articles about (3S,5S)-1-((S)-4-benzyl-2-thioxothiazolidin-3-yl)-5-(tert-butyldimethylsilyloxy)-7-(4-(tert-butyldimethylsilyloxy)phenyl)-3-hydroxyheptan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

(S)-3-(tert-butyl-dimethyl-silanyloxy)-5-[4-(tert-butyl-dimethyl-silanyloxy)phenyl]pentanal (1068608-43-4) + (S)-1-(4-benzyl-2-thioxothiazolidin-3-yl)ethan-1-one (790661-41-5) → C35H55NO4S2Si2 + (3S,5S)-1-((S)-4-benzyl-2-thioxothiazolidin-3-yl)-5-(tert-butyldimethylsilyloxy)-7-(4-(tert-butyldimethylsilyloxy)phenyl)-3-hydroxyheptan-1-one (1068608-46-7)

Guidance literature:

With titanium chloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 ℃;

DOI:10.1016/j.tetlet.2008.07.027

Reference yield: 76.0%

(3S,5S)-1-((S)-4-benzyl-2-thioxothiazolidin-3-yl)-5-(tert-butyldimethylsilyloxy)-7-(4-(tert-butyldimethylsilyloxy)phenyl)-3-hydroxyheptan-1-one (1068608-46-7) + chloromethyl methyl ether (107-30-2) → C37H59NO5S2Si2 (1068608-32-1)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 ℃;

DOI:10.1016/j.tetlet.2008.07.027

upstream raw materials:

(S)-3-(tert-butyl-dimethyl-silanyloxy)-5-[4-(tert-butyl-dimethyl-silanyloxy)phenyl]pentanal

(S)-1-(4-benzyl-2-thioxothiazolidin-3-yl)ethan-1-one

Downstream raw materials:

C₃₇H₅₉NO₅S₂Si₂

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