C₄₁H₅₅FN₄O₇

Base Information

Chemical Name:C₄₁H₅₅FN₄O₇
CAS No.:524018-35-7
Molecular Formula:C₄₁H₅₅FN₄O₇
Molecular Weight:734.909
Hs Code.:

C<sub>41</sub>H<sub>55</sub>FN<sub>4</sub>O<sub>7</sub>

Synonyms:C₄₁H₅₅FN₄O₇

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Chemical Property of C₄₁H₅₅FN₄O₇

Chemical Property:

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Technology Process of C₄₁H₅₅FN₄O₇

There total 7 articles about C₄₁H₅₅FN₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 524018-08-4
[1-(4-oxo-3,4-dihydro-2H-pyran-2-yl)-2-phenyl-ethyl]-carbamic acid tert-butyl ester

: 524018-35-7
C₄₁H₅₅FN₄O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: 70 percent / Br₂; Et₃N / CCl₄ / 1 h / 20 °C

2.1: 61 percent / Na₂CO₃ / tetrakis triphenylphosphinepalladium / benzene; H₂O / 3 h / Heating

3.1: 83 percent / L-Selecrtide / tetrahydrofuran / 0.5 h / -78 °C

4.1: NaH / tetrahydrofuran / 1 h / 0 °C

4.2: 90 percent / tetrahydrofuran / 3 h / -40 °C

5.1: H₂; NaBH₄ / PdCl₂ / ethanol

6.1: NH₄OH; H₂ / Raney nickel / methanol / 2068.59 Torr

7.1: 0.012 g / HgCl₂; Et₃N / dimethylformamide / 2 h / 0 °C

With ammonium hydroxide; sodium tetrahydroborate; hydrogen; bromine; L-Selectride; sodium hydride; sodium carbonate; triethylamine; mercury dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; nickel; palladium dichloride; In tetrahydrofuran; methanol; tetrachloromethane; ethanol; water; N,N-dimethyl-formamide; benzene; 2.1: Suzuki coupling / 4.2: Horner-Emmons reaction;
DOI:10.1021/ol027281v

Reference yield:

: 524018-10-8
[1-(5-bromo-4-oxo-3,4-dihydro-2H-pyran-2-yl)-2-phenyl-ethyl]-carbamic acid tert-butyl ester

: 524018-35-7
C₄₁H₅₅FN₄O₇

Guidance literature:: Multi-step reaction with 6 steps

1.1: 61 percent / Na₂CO₃ / tetrakis triphenylphosphinepalladium / benzene; H₂O / 3 h / Heating

2.1: 83 percent / L-Selecrtide / tetrahydrofuran / 0.5 h / -78 °C

3.1: NaH / tetrahydrofuran / 1 h / 0 °C

3.2: 90 percent / tetrahydrofuran / 3 h / -40 °C

4.1: H₂; NaBH₄ / PdCl₂ / ethanol

5.1: NH₄OH; H₂ / Raney nickel / methanol / 2068.59 Torr

6.1: 0.012 g / HgCl₂; Et₃N / dimethylformamide / 2 h / 0 °C

With ammonium hydroxide; sodium tetrahydroborate; hydrogen; L-Selectride; sodium hydride; sodium carbonate; triethylamine; mercury dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; nickel; palladium dichloride; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide; benzene; 1.1: Suzuki coupling / 3.2: Horner-Emmons reaction;
DOI:10.1021/ol027281v

Reference yield:

: 524018-19-7
[2-(4-fluoro-phenyl)-1-(5-naphthalen-2-yl-4-oxo-tetrahydro-pyran-2-yl)-ethyl]carbamic acid tert-butyl ester

: 524018-35-7
C₄₁H₅₅FN₄O₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaH / tetrahydrofuran / 1 h / 0 °C

1.2: 90 percent / tetrahydrofuran / 3 h / -40 °C

2.1: H₂; NaBH₄ / PdCl₂ / ethanol

3.1: NH₄OH; H₂ / Raney nickel / methanol / 2068.59 Torr

4.1: 0.012 g / HgCl₂; Et₃N / dimethylformamide / 2 h / 0 °C

With ammonium hydroxide; sodium tetrahydroborate; hydrogen; sodium hydride; triethylamine; mercury dichloride; nickel; palladium dichloride; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; 1.2: Horner-Emmons reaction;
DOI:10.1021/ol027281v