5,5'-(1-(3-(azacyclotridecan-1-yl)propyl)-1H-pyrrole-3,4-diyl)bis(3-nitrobenzene-1,2-diol)

Base Information

Chemical Name:5,5'-(1-(3-(azacyclotridecan-1-yl)propyl)-1H-pyrrole-3,4-diyl)bis(3-nitrobenzene-1,2-diol)
CAS No.:1561902-73-5
Molecular Formula:C₃₁H₄₀N₄O₈
Molecular Weight:596.681
Hs Code.:

Synonyms:5,5'-(1-(3-(azacyclotridecan-1-yl)propyl)-1H-pyrrole-3,4-diyl)bis(3-nitrobenzene-1,2-diol)

Suppliers and Price of 5,5'-(1-(3-(azacyclotridecan-1-yl)propyl)-1H-pyrrole-3,4-diyl)bis(3-nitrobenzene-1,2-diol)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5,5'-(1-(3-(azacyclotridecan-1-yl)propyl)-1H-pyrrole-3,4-diyl)bis(3-nitrobenzene-1,2-diol)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5,5'-(1-(3-(azacyclotridecan-1-yl)propyl)-1H-pyrrole-3,4-diyl)bis(3-nitrobenzene-1,2-diol)

There total 13 articles about 5,5'-(1-(3-(azacyclotridecan-1-yl)propyl)-1H-pyrrole-3,4-diyl)bis(3-nitrobenzene-1,2-diol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1561902-66-6
C₃₃H₄₄N₄O₈

: 1561902-73-5
5,5'-(1-(3-(azacyclotridecan-1-yl)propyl)-1H-pyrrole-3,4-diyl)bis(3-nitrobenzene-1,2-diol)

Guidance literature:: With boron tribromide; In dichloromethane; for 0.5h; Inert atmosphere;

Reference yield: 12.0%

: 1561902-66-6
C₃₃H₄₄N₄O₈

: 1561902-70-2
C₃₂H₄₂N₄O₈

: 1561902-73-5
5,5'-(1-(3-(azacyclotridecan-1-yl)propyl)-1H-pyrrole-3,4-diyl)bis(3-nitrobenzene-1,2-diol)

Guidance literature:: With boron tribromide; In dichloromethane; at -78 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c3ob42309c

Reference yield:

: 295-03-4
azacyclotridecane

: 1561902-73-5
5,5'-(1-(3-(azacyclotridecan-1-yl)propyl)-1H-pyrrole-3,4-diyl)bis(3-nitrobenzene-1,2-diol)

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / N,N-dimethyl-formamide / 16 h / 70 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / diethyl ether / 0.25 h / 0 - 33 °C / Inert atmosphere

3.1: sodium iodide / dimethyl sulfoxide / 0.25 h / Inert atmosphere

3.2: 16 h

4.1: boron tribromide / dichloromethane / 0.5 h / Inert atmosphere

With lithium aluminium tetrahydride; boron tribromide; triethylamine; sodium iodide; In diethyl ether; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;