Methyl 3,4-dimethoxyphenyldithiocarboxylate

Base Information

• Chemical Name: Methyl 3,4-dimethoxyphenyldithiocarboxylate
• CAS No.: 69922-38-9
• Molecular Formula: C₁₀H₁₂O₂S₂
• Molecular Weight: 228.336

Synonyms:Methyl 3,4-dimethoxyphenyldithiocarboxylate

Chemical Property of Methyl 3,4-dimethoxyphenyldithiocarboxylate

Chemical Property:

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Technology Process of Methyl 3,4-dimethoxyphenyldithiocarboxylate

There total 1 articles about Methyl 3,4-dimethoxyphenyldithiocarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ Methyl 3,4-dimethoxyphenyldithiocarboxylate (69922-38-9)

Guidance literature:

Verb./BRN= 846494/, NaH, HMPA;

Reference yield: 94.0%

Methyl 3,4-dimethoxyphenyldithiocarboxylate (69922-38-9) + C8H9ClN2O → 2-(3,4-dimethoxyphenyl)-5-(4-methoxyphenyl)-1,3,4-thiadiazole

Guidance literature:

With triethylamine; In ethanol; for 48h; Reflux;

DOI:10.1080/00397911.2020.1745843

Reference yield: 92.0%

[(p-methylphenyl)sulfonylmethyl]isonitrile (38622-91-2,36635-61-7) + Methyl 3,4-dimethoxyphenyldithiocarboxylate (69922-38-9) → 5-(3,4-dimethoxyphenyl)-4-[(4-methylphenyl)sulfonyl]thiazole (1384515-61-0)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 0.25h;

DOI:10.1055/s-0031-1290762

Downstream raw materials:

2-Cyano-3-(3,4-dimethoxyphenyl)-3-methylthioacrylonitrile

5-(3,4-dimethoxyphenyl)-4-phenylthiazole

5-(3,4-dimethoxyphenyl)-4-[(4-methylphenyl)sulfonyl]thiazole

(Z)-4-[(3,4-dimethoxyphenyl)(methylthio)methylene]-2-phenyloxazol-5(4H)-one

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