Technology Process of C26H26ClN5O3
There total 11 articles about C26H26ClN5O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium diacetate; triethylamine; triphenylphosphine;
In
acetonitrile;
at 70 ℃;
for 3h;
Sealed tube;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: N-Bromosuccinimide / 1,2-dichloro-ethane / 1 h / Reflux
2: titanium tetrachloride / tetrahydrofuran; dichloromethane / 41.5 h / 0 - 20 °C
3: potassium carbonate / N,N-dimethyl-formamide / 3 h / 50 °C
4: potassium carbonate / N,N-dimethyl-formamide / 2 h / 50 °C
5: triethylamine; palladium diacetate; triphenylphosphine / acetonitrile / 3 h / 70 °C / Sealed tube
With
N-Bromosuccinimide; palladium diacetate; titanium tetrachloride; potassium carbonate; triethylamine; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: titanium tetrachloride / tetrahydrofuran; dichloromethane / 41.5 h / 0 - 20 °C
2: potassium carbonate / N,N-dimethyl-formamide / 3 h / 50 °C
3: potassium carbonate / N,N-dimethyl-formamide / 2 h / 50 °C
4: triethylamine; palladium diacetate; triphenylphosphine / acetonitrile / 3 h / 70 °C / Sealed tube
With
palladium diacetate; titanium tetrachloride; potassium carbonate; triethylamine; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
