1,20-Bis-(4-benzyloxy-phenyl)-6,9,12,15-tetraoxa-3,18-diaza-tricyclo[16.3.1.1^3,20]tricosan-21-one

Base Information

• Chemical Name: 1,20-Bis-(4-benzyloxy-phenyl)-6,9,12,15-tetraoxa-3,18-diaza-tricyclo[16.3.1.1^3,20]tricosan-21-one
• CAS No.: 157108-65-1
• Molecular Formula: C₄₃H₅₀N₂O₇
• Molecular Weight: 706.879

Synonyms:1,20-Bis-(4-benzyloxy-phenyl)-6,9,12,15-tetraoxa-3,18-diaza-tricyclo[16.3.1.1^3,20]tricosan-21-one

Chemical Property of 1,20-Bis-(4-benzyloxy-phenyl)-6,9,12,15-tetraoxa-3,18-diaza-tricyclo[16.3.1.1^3,20]tricosan-21-one

Chemical Property:

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Technology Process of 1,20-Bis-(4-benzyloxy-phenyl)-6,9,12,15-tetraoxa-3,18-diaza-tricyclo[16.3.1.1^3,20]tricosan-21-one

There total 1 articles about 1,20-Bis-(4-benzyloxy-phenyl)-6,9,12,15-tetraoxa-3,18-diaza-tricyclo[16.3.1.1^3,20]tricosan-21-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

1,5-Bis-(4-benzyloxy-benzyl)-3,7-bis-(2-hydroxy-ethyl)-3,7-diaza-bicyclo[3.3.1]nonan-9-one + triethylene glycol di-(p-toluenesulfonate) (19249-03-7) → 1,20-Bis-(4-benzyloxy-phenyl)-6,9,12,15-tetraoxa-3,18-diaza-tricyclo[16.3.1.13,20]tricosan-21-one (157108-65-1)

Guidance literature:

With sodium hydride; In tetrahydrofuran; Heating;

DOI:10.1021/ja00030a077

Reference yield: 73.0%

1,20-Bis-(4-benzyloxy-phenyl)-6,9,12,15-tetraoxa-3,18-diaza-tricyclo[16.3.1.13,20]tricosan-21-one (157108-65-1) → 1,20-Bis-(4-hydroxy-phenyl)-6,9,12,15-tetraoxa-3,18-diaza-tricyclo[16.3.1.13,20]tricosan-21-one (138434-76-1)

Guidance literature:

With ammonium formate; palladium on activated charcoal; In acetone; Heating;

DOI:10.1021/ja00030a077

Reference yield:

1,20-Bis-(4-benzyloxy-phenyl)-6,9,12,15-tetraoxa-3,18-diaza-tricyclo[16.3.1.13,20]tricosan-21-one (157108-65-1) → 1,20-Bis-[4-(4-chloro-butoxy)-phenyl]-6,9,12,15-tetraoxa-3,18-diaza-tricyclo[16.3.1.13,20]tricosan-21-one (138434-81-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 73 percent / HCOONH₄ / 10percent Pd/C / acetone / Heating

2: 99 percent / NaH / dimethylformamide / 20 °C

With ammonium formate; sodium hydride; palladium on activated charcoal; In N,N-dimethyl-formamide; acetone;

DOI:10.1021/ja00030a077

upstream raw materials:

triethylene glycol di-(p-toluenesulfonate)

Downstream raw materials:

1,20-Bis-(4-hydroxy-phenyl)-6,9,12,15-tetraoxa-3,18-diaza-tricyclo[16.3.1.1^3,20]tricosan-21-one

1,20-Bis-[4-(4-chloro-butoxy)-phenyl]-6,9,12,15-tetraoxa-3,18-diaza-tricyclo[16.3.1.1^3,20]tricosan-21-one

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