C₁₆H₂₄O₃

Base Information

Chemical Name:C₁₆H₂₄O₃
CAS No.:1394985-36-4
Molecular Formula:C₁₆H₂₄O₃
Molecular Weight:264.365
Hs Code.:

C<sub>16</sub>H<sub>24</sub>O<sub>3</sub>

Synonyms:C₁₆H₂₄O₃

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Chemical Property of C₁₆H₂₄O₃

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Technology Process of C₁₆H₂₄O₃

There total 1 articles about C₁₆H₂₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 189069-40-7
(2S,3S,4S)-2,4-Dimethyl-hexane-1,3-diol

: 1394985-36-4
C₁₆H₂₄O₃

Guidance literature:: With pyridinium p-toluenesulfonate; In dichloromethane; at 20 - 25 ℃; Inert atmosphere;
DOI:10.1039/c2cc34187e

Reference yield: 97.0%

: 1394985-36-4
C₁₆H₂₄O₃

: 1394985-55-7
C₁₆H₂₆O₃

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; at -78 - -10 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c2cc34187e

Reference yield:

: 1394985-36-4
C₁₆H₂₄O₃

: C₄₉H₈₁N₅O₁₁

Guidance literature:: Multi-step reaction with 11 steps

1.1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 - -10 °C / Inert atmosphere

2.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 °C / Inert atmosphere

3.1: boron trifluoride diethyl etherate / dichloromethane / 2 h / -78 °C / Inert atmosphere

4.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere

5.1: 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide / 1,4-dioxane; water; tert-butyl alcohol / 20 - 25 °C / Inert atmosphere

6.1: N-ethyl-N,N-diisopropylamine; lithium chloride / acetonitrile / 0.33 h / 20 - 25 °C / Inert atmosphere

6.2: 20 h / 20 - 25 °C / Inert atmosphere

7.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.17 h / 20 - 25 °C / pH 7.1 / Inert atmosphere; aq. phosphate buffer

8.1: dmap / toluene / 8 h / 0 - 60 °C / Inert atmosphere

9.1: diethylamine / acetonitrile / 1 h / 0 - 20 °C / Inert atmosphere

10.1: 1-hydroxy-7-aza-benzotriazole; HATU / N,N-dimethyl-formamide / 14 h / 0 - 20 °C / Inert atmosphere

11.1: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; dmap; sodium periodate; osmium(VIII) oxide; 1-hydroxy-7-aza-benzotriazole; boron trifluoride diethyl etherate; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; diethylamine; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium chloride; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; tert-butyl alcohol; 6.2: Horner-Wadsworth-Emmons olefination;
DOI:10.1039/c2cc34187e