C₅₈H₈₁N₁₃O₁₄

Base Information

Chemical Name:C₅₈H₈₁N₁₃O₁₄
CAS No.:1203557-38-3
Molecular Formula:C₅₈H₈₁N₁₃O₁₄
Molecular Weight:1184.36
Hs Code.:

C<sub>58</sub>H<sub>81</sub>N<sub>13</sub>O<sub>14</sub>

Synonyms:C₅₈H₈₁N₁₃O₁₄

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Chemical Property of C₅₈H₈₁N₁₃O₁₄

Chemical Property:

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Technology Process of C₅₈H₈₁N₁₃O₁₄

There total 10 articles about C₅₈H₈₁N₁₃O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1203557-76-9
C₂₄H₃₄N₆O₈

: C₃₄H₄₉N₇O₇

: 1203557-38-3
C₅₈H₈₁N₁₃O₁₄

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 10h;
DOI:10.1016/j.ejmech.2012.01.054

Reference yield:

: 84520-67-2
(2S,4R)-4-(methylsulfonyloxy)pyrrolidine-1,2-dicarboxylic acid 1-tert-butylester-2-methylester

: 1203557-38-3
C₅₈H₈₁N₁₃O₁₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium azide / N,N-dimethyl-formamide / 24 h / 60 °C

2.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.33 h / 0 °C

3.2: 25 h / 0 - 20 °C

4.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 24.67 h / 0 - 20 °C

6.1: sodium hydroxide / ethanol / 24 h / 20 °C

6.2: pH 4.5

7.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 10 h / 20 °C

With sodium azide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.01.054

Reference yield:

: 772327-98-7
(2S,4S)-1-((2S,3R)-2-Amino-3-hydroxy-butyryl)-4-azido-pyrrolidine-2-carboxylic acid methyl ester

: 1203557-38-3
C₅₈H₈₁N₁₃O₁₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 24.67 h / 0 - 20 °C

2.1: sodium hydroxide / ethanol / 24 h / 20 °C

2.2: pH 4.5

3.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 10 h / 20 °C

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In ethanol; dichloromethane;
DOI:10.1016/j.ejmech.2012.01.054