(1R,3R,5S)-bicyclo[3.3.1]nonan-3-amine diphenyl phosphate salt

Base Information

Chemical Name:(1R,3R,5S)-bicyclo[3.3.1]nonan-3-amine diphenyl phosphate salt
CAS No.:1384190-00-4
Molecular Formula:C₉H₁₇N*C₁₂H₁₁O₄P
Molecular Weight:389.431
Hs Code.:

Synonyms:(1R,3R,5S)-bicyclo[3.3.1]nonan-3-amine diphenyl phosphate salt

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Chemical Property of (1R,3R,5S)-bicyclo[3.3.1]nonan-3-amine diphenyl phosphate salt

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Technology Process of (1R,3R,5S)-bicyclo[3.3.1]nonan-3-amine diphenyl phosphate salt

There total 7 articles about (1R,3R,5S)-bicyclo[3.3.1]nonan-3-amine diphenyl phosphate salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 26386-88-9
diphenyl phosphoryl azide

: 19489-16-8
(1R,3r,5S)-bicyclo[3.3.1]nonane-3-carboxylic acid

: 1384190-00-4
(1R,3R,5S)-bicyclo[3.3.1]nonan-3-amine diphenyl phosphate salt

Guidance literature:: diphenyl phosphoryl azide; (1R,3r,5S)-bicyclo[3.3.1]nonane-3-carboxylic acid; With triethylamine; In toluene; at 25 - 75 ℃; Inert atmosphere;

With sodium hydroxide; In tetrahydrofuran; water; at 0 - 5 ℃; for 1.25h;

Reference yield:

: 700-58-3
2-Adamantanone

: 1384190-00-4
(1R,3R,5S)-bicyclo[3.3.1]nonan-3-amine diphenyl phosphate salt

Guidance literature:: Multi-step reaction with 5 steps

1.1: trifluoroacetic acid; sodium percarbonate / 3 h / 20 - 60 °C / Industry scale

2.1: sodium hydroxide; water / methanol / 36 h / Reflux; Industry scale

2.2: pH ~ 2.5 / Industry scale

3.1: methanesulfonic acid / 5 h / Reflux; Industry scale

4.1: hydrogen / palladium 10% on activated carbon / methanol / 2585.81 Torr / Industry scale

5.1: triethylamine / toluene / 75 - 90 °C / Inert atmosphere; Industry scale

5.2: 19 h / 0 - 5 °C / Industry scale

5.3: pH ~ 6 - ~ 7 / Industry scale

With sodium percarbonate; water; hydrogen; triethylamine; trifluoroacetic acid; sodium hydroxide; methanesulfonic acid; palladium 10% on activated carbon; In methanol; toluene;

Reference yield:

: 87860-03-5
(1R,3r,5S,7r)-7-hydroxybicyclo[3.3.1]nonane-3-carboxylic acid

: 1384190-00-4
(1R,3R,5S)-bicyclo[3.3.1]nonan-3-amine diphenyl phosphate salt

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanesulfonic acid / 5 h / Reflux; Industry scale

2.1: hydrogen / palladium 10% on activated carbon / methanol / 2585.81 Torr / Industry scale

3.1: triethylamine / toluene / 75 - 90 °C / Inert atmosphere; Industry scale

3.2: 19 h / 0 - 5 °C / Industry scale

3.3: pH ~ 6 - ~ 7 / Industry scale

With hydrogen; triethylamine; methanesulfonic acid; palladium 10% on activated carbon; In methanol; toluene;