N⁶-Benzoyl-9-(4',6'-di-O-benzoyl-2',3'-dideoxy-β-D-glucopyranosyl)adenin

Base Information

Chemical Name:N⁶-Benzoyl-9-(4',6'-di-O-benzoyl-2',3'-dideoxy-β-D-glucopyranosyl)adenin
CAS No.:145593-80-2
Molecular Formula:C₃₂H₂₇N₅O₆
Molecular Weight:577.596
Hs Code.:

N<sup>6</sup>-Benzoyl-9-(4',6'-di-O-benzoyl-2',3'-dideoxy-β-D-glucopyranosyl)adenin

Synonyms:N⁶-Benzoyl-9-(4',6'-di-O-benzoyl-2',3'-dideoxy-β-D-glucopyranosyl)adenin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N⁶-Benzoyl-9-(4',6'-di-O-benzoyl-2',3'-dideoxy-β-D-glucopyranosyl)adenin

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Technology Process of N⁶-Benzoyl-9-(4',6'-di-O-benzoyl-2',3'-dideoxy-β-D-glucopyranosyl)adenin

There total 5 articles about N⁶-Benzoyl-9-(4',6'-di-O-benzoyl-2',3'-dideoxy-β-D-glucopyranosyl)adenin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 145593-73-3
(+)-[(2R,3S,6S)-2-(benzoyloxymethyl)-6-methoxyoxan-3-yl] benzoate

: 4005-49-6
N-benzoyladenine

: 145593-81-3
N⁶-Benzoyl-9-(4',6'-di-O-benzoyl-2',3'-dideoxy-α-D-glucopyranosyl)adenin

: 145593-80-2
N⁶-Benzoyl-9-(4',6'-di-O-benzoyl-2',3'-dideoxy-β-D-glucopyranosyl)adenin

Guidance literature:: With chloro-trimethyl-silane; tin(IV) chloride; 1,1,1,3,3,3-hexamethyl-disilazane; In acetonitrile; for 20h; Yields of byproduct given; Ambient temperature;
DOI:10.1002/hlca.19920750503

Reference yield:

: 3427-20-1
methyl 4,6-di-O-acetyl-2,3-dideoxy-D-erythro-hex-2-enopyranoside

: 145593-80-2
N⁶-Benzoyl-9-(4',6'-di-O-benzoyl-2',3'-dideoxy-β-D-glucopyranosyl)adenin

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / H₂, AcOH / 10percent Pd/C / methanol / 8 h / Ambient temperature

2: Amberlit IRA 400 (OH^--Form) / methanol / 2 h / Ambient temperature

3: pyridine / r.t.

4: 35 percent / 1a) hexamethyldisilazane, 1b) chlorotrimethylsilane, 2) SnCl₄ / acetonitrile / 20 h / Ambient temperature

With pyridine; chloro-trimethyl-silane; hydrogen; tin(IV) chloride; acetic acid; 1,1,1,3,3,3-hexamethyl-disilazane; palladium on activated charcoal; Amberlit IRA 400 (OH^--Form); In methanol; acetonitrile;
DOI:10.1002/hlca.19920750503

Reference yield:

: 23339-17-5
methyl 4,6-di-O-acetyl-2,3-dideoxy-D-erythro-hexopyranoside

: 145593-80-2
N⁶-Benzoyl-9-(4',6'-di-O-benzoyl-2',3'-dideoxy-β-D-glucopyranosyl)adenin

Guidance literature:: Multi-step reaction with 3 steps

1: Amberlit IRA 400 (OH^--Form) / methanol / 2 h / Ambient temperature

2: pyridine / r.t.

3: 35 percent / 1a) hexamethyldisilazane, 1b) chlorotrimethylsilane, 2) SnCl₄ / acetonitrile / 20 h / Ambient temperature

With pyridine; chloro-trimethyl-silane; tin(IV) chloride; 1,1,1,3,3,3-hexamethyl-disilazane; Amberlit IRA 400 (OH^--Form); In methanol; acetonitrile;
DOI:10.1002/hlca.19920750503