O₂-methyl 1-[4-(propargyloxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diolate

Base Information

• Chemical Name: O₂-methyl 1-[4-(propargyloxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diolate
• CAS No.: 1246199-56-3
• Molecular Formula: C₉H₁₄N₄O₄
• Molecular Weight: 242.235

Synonyms:O₂-methyl 1-[4-(propargyloxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diolate

Chemical Property of O₂-methyl 1-[4-(propargyloxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diolate

Chemical Property:

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Technology Process of O₂-methyl 1-[4-(propargyloxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diolate

There total 1 articles about O₂-methyl 1-[4-(propargyloxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

propargyl chloroformate (35718-08-2) + O2-methyl 1-(piperazin-1-yl)diazen-1-ium-1,2-diolate (178948-51-1,960233-38-9) → O2-methyl 1-[4-(propargyloxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diolate (1246199-56-3)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1021/ol101645k

Reference yield: 74.0%

5,5-di(azidomethyl)-2-phenyl-1,3-dioxane (104274-83-1) + O2-methyl 1-[4-(propargyloxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diolate (1246199-56-3) → [OA-1-120] (1246199-60-9)

Guidance literature:

With copper(l) iodide; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃;

DOI:10.1021/ol101645k

Reference yield: 60.0%

5,5-di(azidomethyl)-2-phenyl-1,3-dioxane (104274-83-1) + O2-methyl 1-[4-(propargyloxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diolate (1246199-56-3) → [OA-1-112] (1246199-59-6) + [OA-1-120] (1246199-60-9)

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; water; at 20 ℃;

DOI:10.1021/ol101645k

upstream raw materials:

propargyl chloroformate

O₂-methyl 1-(piperazin-1-yl)diazen-1-ium-1,2-diolate

Downstream raw materials:

[OA-1-112]

[OA-1-120]

[OA-1-128]

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