1-benzyl-4-(5-fluoro-3-methyl-1H-indol-2-yl)-N,N-dimethylcyclohexanamine

Base Information

Chemical Name:1-benzyl-4-(5-fluoro-3-methyl-1H-indol-2-yl)-N,N-dimethylcyclohexanamine
CAS No.:1004542-39-5
Molecular Formula:C₂₄H₂₉FN₂
Molecular Weight:364.506
Hs Code.:

Synonyms:1-benzyl-4-(5-fluoro-3-methyl-1H-indol-2-yl)-N,N-dimethylcyclohexanamine

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Chemical Property of 1-benzyl-4-(5-fluoro-3-methyl-1H-indol-2-yl)-N,N-dimethylcyclohexanamine

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Technology Process of 1-benzyl-4-(5-fluoro-3-methyl-1H-indol-2-yl)-N,N-dimethylcyclohexanamine

There total 4 articles about 1-benzyl-4-(5-fluoro-3-methyl-1H-indol-2-yl)-N,N-dimethylcyclohexanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1004541-70-1
(+/-)-2-(4-(dimethylamino)-4-phenylcyclohex-1-enyl)-3-methyl-5-trifluoromethyl-1H-indole, citrate

: 1004542-41-9
1-benzyl-4-(5-fluoro-3-methyl-1H-indol-2-yl)-N,N-dimethylcyclohexanamine

: 1004542-39-5
1-benzyl-4-(5-fluoro-3-methyl-1H-indol-2-yl)-N,N-dimethylcyclohexanamine

Guidance literature:: With hydrogen; 5%-palladium/activated carbon; In methanol; at 20 ℃; for 2h; under 2250.23 Torr;

Reference yield:

: 392-13-2
5-fluoro-3-methyl-1H-indole

: 1004542-39-5
1-benzyl-4-(5-fluoro-3-methyl-1H-indol-2-yl)-N,N-dimethylcyclohexanamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluorormethanesulfonic acid / dichloromethane / 22 h / 20 °C

1.2: 0.33 h

2.1: methanol

3.1: hydrogen / 5%-palladium/activated carbon / methanol / 2 h / 20 °C / 2250.23 Torr

With trifluorormethanesulfonic acid; hydrogen; 5%-palladium/activated carbon; In methanol; dichloromethane;

Reference yield:

: 475098-34-1
4-benzyl-4-(dimethylamino)cyclohexanone

: 1004542-39-5
1-benzyl-4-(5-fluoro-3-methyl-1H-indol-2-yl)-N,N-dimethylcyclohexanamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluorormethanesulfonic acid / dichloromethane / 22 h / 20 °C

1.2: 0.33 h

2.1: methanol

3.1: hydrogen / 5%-palladium/activated carbon / methanol / 2 h / 20 °C / 2250.23 Torr

With trifluorormethanesulfonic acid; hydrogen; 5%-palladium/activated carbon; In methanol; dichloromethane;