(E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-methyl-6-triisopropylsilyloxyhex-2-enyl ester

Base Information

Chemical Name:(E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-methyl-6-triisopropylsilyloxyhex-2-enyl ester
CAS No.:960060-48-4
Molecular Formula:C₂₅H₄₀F₃NO₃Si
Molecular Weight:487.678
Hs Code.:

Synonyms:(E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-methyl-6-triisopropylsilyloxyhex-2-enyl ester

Suppliers and Price of (E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-methyl-6-triisopropylsilyloxyhex-2-enyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-methyl-6-triisopropylsilyloxyhex-2-enyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-methyl-6-triisopropylsilyloxyhex-2-enyl ester

There total 1 articles about (E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-methyl-6-triisopropylsilyloxyhex-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 960060-27-9
(E)-3-methyl-6-((triisopropylsilyl)oxy)hex-2-en-1-ol

: 75999-66-5
N-(4-methoxyphenyl)trifluoroacetimidoyl chloride

: 960060-48-4
(E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-methyl-6-triisopropylsilyloxyhex-2-enyl ester

Guidance literature:: (E)-3-methyl-6-((triisopropylsilyl)oxy)hex-2-en-1-ol; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.0833333h; Inert atmosphere;

N-(4-methoxyphenyl)trifluoroacetimidoyl chloride; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1002/chem.200900712

Reference yield: 73.0%

: 960060-48-4
(E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-methyl-6-triisopropylsilyloxyhex-2-enyl ester

: 960060-62-2
(R)-2,2,2-trifluoro-N-(4-methoxyphenyl)-N-(3-triisopropylsilyloxypropyl-1-methyl-1-allyl)acetamid

Guidance literature:: With di-μ-chlorobis[η⁵-(4'R,5'R)-(S_p)-2-(2'-4',5'-dihydro-4',5'-diphenyl-1'-tosyl-1'H-imidazolyl)cyclopentadienyl, (1-C,3'-N)(η⁵-pentaphenylcyclopentadienyl)-iron(II)]dipalladium(II); silver trifluoroacetate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; In dichloromethane; at 50 ℃; for 60h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/chem.200900712