(carbonyl)3cobalt(μ-PhC2CH2(tungsten)(carbonyl)3Cp)cobalt(carbonyl)3

Base Information

Chemical Name:(carbonyl)3cobalt(μ-PhC2CH2(tungsten)(carbonyl)3Cp)cobalt(carbonyl)3
CAS No.:111635-12-2
Molecular Formula:C₂₃H₁₂Co₂O₉W
Molecular Weight:734.179
Hs Code.:

Synonyms:(carbonyl)3cobalt(μ-PhC2CH2(tungsten)(carbonyl)3Cp)cobalt(carbonyl)3

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Chemical Property of (carbonyl)3cobalt(μ-PhC2CH2(tungsten)(carbonyl)3Cp)cobalt(carbonyl)3

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Technology Process of (carbonyl)3cobalt(μ-PhC2CH2(tungsten)(carbonyl)3Cp)cobalt(carbonyl)3

There total 1 articles about (carbonyl)3cobalt(μ-PhC2CH2(tungsten)(carbonyl)3Cp)cobalt(carbonyl)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 32993-03-6
tungsten(carbonyl)3CH₂CCPh

: 111635-12-2
(carbonyl)3cobalt(μ-PhC2CH2(tungsten)(carbonyl)3Cp)cobalt(carbonyl)3

Guidance literature:: In pentane; Addn. of W-complex soln. to Co2(CO)8 soln. under inert gas with stirring over 15 min, gas is evolved, stirring (1 h).; Evapn. in vac., yields purple cryst. residue, column chromy. (Florisil, pentane), band is collected, evapn. to dryness, elem. anal.;

Reference yield: 63.0%

: 111635-12-2
(carbonyl)3cobalt(μ-PhC2CH2(tungsten)(carbonyl)3Cp)cobalt(carbonyl)3

: 76-05-1
trifluoroacetic acid

: {WCo(μ-CH3CCPh)(CO)5(η-C5H5)}

Guidance literature:: In dichloromethane; Addn. of CF3COOH to trinuclear WCo2-complex soln. under inert gas, stirring (8 h, room temp.), gas evolution is observed as the purple soln. turns red.; Filtn. of a red powder, column chromy. (Florisil, petroleum ether-diethyl ether) of the filtrate gives red band, evapn. to dryness, crystn. (pentane).;

Reference yield: 56.0%

: 111635-12-2
(carbonyl)3cobalt(μ-PhC2CH2(tungsten)(carbonyl)3Cp)cobalt(carbonyl)3

: {WCo(μ-CH3CCPh)(CO)5(η-C5H5)}

Guidance literature:: With Al₂O₃; In pentane; Addn. of alumina to trinuclear WCo2-complex soln. under inert gas, stirring (9 h, room temp.), gas evolution is observed as the dark purple soln. turns red.; Filtn., washing (diethyl ether), combination of filtrate and washings, evapn., column chromy. (Florisil, petroleum ether-diethyl ether) gives red band, evapn. to dryness, crystn. (pentane), elem. anal., mol. wt.;