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Technology Process of Ti(1,2-alternate dimethylsilyl-bridged p-tert-butylcalix[4]arene dianion)(OC(p-MeC6H3)2C4tBu(SiMe3)H2)

Ti(1,2-alternate dimethylsilyl-bridged p-tert-butylcalix[4]arene dianion)(OC(p-MeC6H3)2C4tBu(SiMe3)H2)

Base Information
  • Chemical Name:Ti(1,2-alternate dimethylsilyl-bridged p-tert-butylcalix[4]arene dianion)(OC(p-MeC6H3)2C4tBu(SiMe3)H2)
  • CAS No.:475975-35-0
  • Molecular Formula:C72H92O5Si2Ti
  • Molecular Weight:1141.57
  • Hs Code.:
Ti(1,2-alternate dimethylsilyl-bridged p-tert-butylcalix[4]arene dianion)(OC(p-MeC<sub>6</sub>H<sub>3</sub>)2C<sub>4</sub>tBu(SiMe<sub>3</sub>)H<sub>2</sub>)

Synonyms:Ti(1,2-alternate dimethylsilyl-bridged p-tert-butylcalix[4]arene dianion)(OC(p-MeC6H3)2C4tBu(SiMe3)H2)

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Chemical Property of Ti(1,2-alternate dimethylsilyl-bridged p-tert-butylcalix[4]arene dianion)(OC(p-MeC6H3)2C4tBu(SiMe3)H2)
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Technology Process of Ti(1,2-alternate dimethylsilyl-bridged p-tert-butylcalix[4]arene dianion)(OC(p-MeC6H3)2C4tBu(SiMe3)H2)

There total 1 articles about Ti(1,2-alternate dimethylsilyl-bridged p-tert-butylcalix[4]arene dianion)(OC(p-MeC6H3)2C4tBu(SiMe3)H2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

Ti(1,2-alternate dimethylsilyl-bridged p-tert-butylcalix[4]arene dianion)(OC(p-MeC<sub>6</sub>H<sub>4</sub>)2C<sub>2</sub>tBuH)

Ti(1,2-alternate dimethylsilyl-bridged p-tert-butylcalix[4]arene dianion)(OC(p-MeC6H4)2C2tBuH)

trimethylsilylacetylene
1066-54-2

trimethylsilylacetylene

Ti(1,2-alternate dimethylsilyl-bridged p-tert-butylcalix[4]arene dianion)(OC(p-MeC<sub>6</sub>H<sub>3</sub>)2C<sub>4</sub>tBu(SiMe<sub>3</sub>)H<sub>2</sub>)
475975-35-0

Ti(1,2-alternate dimethylsilyl-bridged p-tert-butylcalix[4]arene dianion)(OC(p-MeC6H3)2C4tBu(SiMe3)H2)

Guidance literature:
In toluene; ligand and Ti-complex were dissolved in toluene, stirred for 2 ds at room temp. under N2; volatiles were removed under reduced pressure, washed with pentane, dried under vac.; elem. anal.;
DOI:10.1021/ja0271577
upstream raw materials:

trimethylsilylacetylene

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