7-isobutyl-8-oso-2-oxa-9-aza-bicyclo[10.2.2]hexadeca-1⁽¹⁵⁾,12⁽¹⁶⁾,13-triene-6,10-dicarboxylic acid 10-(4-aminomethylbenzylamine) 6-hydroxyamide trifluoroacetic acid salt

Base Information

• Chemical Name: 7-isobutyl-8-oso-2-oxa-9-aza-bicyclo[10.2.2]hexadeca-1⁽¹⁵⁾,12⁽¹⁶⁾,13-triene-6,10-dicarboxylic acid 10-(4-aminomethylbenzylamine) 6-hydroxyamide trifluoroacetic acid salt
• CAS No.: 355150-19-5
• Molecular Formula: C₂HF₃O₂*C₂₈H₃₈N₄O₅
• Molecular Weight: 624.657

Synonyms:7-isobutyl-8-oso-2-oxa-9-aza-bicyclo[10.2.2]hexadeca-1⁽¹⁵⁾,12⁽¹⁶⁾,13-triene-6,10-dicarboxylic acid 10-(4-aminomethylbenzylamine) 6-hydroxyamide trifluoroacetic acid salt

Chemical Property of 7-isobutyl-8-oso-2-oxa-9-aza-bicyclo[10.2.2]hexadeca-1⁽¹⁵⁾,12⁽¹⁶⁾,13-triene-6,10-dicarboxylic acid 10-(4-aminomethylbenzylamine) 6-hydroxyamide trifluoroacetic acid salt

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Technology Process of 7-isobutyl-8-oso-2-oxa-9-aza-bicyclo[10.2.2]hexadeca-1⁽¹⁵⁾,12⁽¹⁶⁾,13-triene-6,10-dicarboxylic acid 10-(4-aminomethylbenzylamine) 6-hydroxyamide trifluoroacetic acid salt

There total 1 articles about 7-isobutyl-8-oso-2-oxa-9-aza-bicyclo[10.2.2]hexadeca-1⁽¹⁵⁾,12⁽¹⁶⁾,13-triene-6,10-dicarboxylic acid 10-(4-aminomethylbenzylamine) 6-hydroxyamide trifluoroacetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4-{[(6-hydroxycarbamoyl-7-isobutyl-8-oso-2-oxa-9-aza-bicyclo[10.2.2]hexadeca-1(15),12(16),13-triene-10-carbonyl)-amino]-methyl}-benzyl)-carbamic acid tert-butyl ester (355150-17-3) + trifluoroacetic acid (76-05-1) → 7-isobutyl-8-oso-2-oxa-9-aza-bicyclo[10.2.2]hexadeca-1(15),12(16),13-triene-6,10-dicarboxylic acid 10-(4-aminomethylbenzylamine) 6-hydroxyamide trifluoroacetic acid salt (355150-19-5)

Guidance literature:

In dichloromethane; at 20 ℃; for 1h;

Reference yield:

BOC-cysteic acid N-hydroxysuccinimide ester + 7-isobutyl-8-oso-2-oxa-9-aza-bicyclo[10.2.2]hexadeca-1(15),12(16),13-triene-6,10-dicarboxylic acid 10-(4-aminomethylbenzylamine) 6-hydroxyamide trifluoroacetic acid salt (355150-19-5) → C36H51N5O8S

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 18h;

Reference yield:

7-isobutyl-8-oso-2-oxa-9-aza-bicyclo[10.2.2]hexadeca-1(15),12(16),13-triene-6,10-dicarboxylic acid 10-(4-aminomethylbenzylamine) 6-hydroxyamide trifluoroacetic acid salt (355150-19-5) + 1,4,7-tris(tert-butoxycarbonylmethyl)-1,4,7,10-tetraazacyclododecane-10-acetic acid (137076-54-1) → C56H88N8O12

Guidance literature:

1,4,7-tris(tert-butoxycarbonylmethyl)-1,4,7,10-tetraazacyclododecane-10-acetic acid; With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 0.25h;

7-isobutyl-8-oso-2-oxa-9-aza-bicyclo[10.2.2]hexadeca-1⁽¹⁵⁾,12⁽¹⁶⁾,13-triene-6,10-dicarboxylic acid 10-(4-aminomethylbenzylamine) 6-hydroxyamide trifluoroacetic acid salt; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 18h;

upstream raw materials:

(4-{[(6-hydroxycarbamoyl-7-isobutyl-8-oso-2-oxa-9-aza-bicyclo[10.2.2]hexadeca-1⁽¹⁵⁾,12⁽¹⁶⁾,13-triene-10-carbonyl)-amino]-methyl}-benzyl)-carbamic acid tert-butyl ester

trifluoroacetic acid

Downstream raw materials:

2-({2-[({N-[3-(2-{[7-(N-hydroxycarbamoyl)(3S,6R,7S)-4-aza-6-(2-methylpropyl)-11-oxa-5-oxobicyclo[10.2.2]hexadeca-1⁽¹⁵⁾,12⁽¹⁶⁾,13-trien-3-yl]carbonylamino}acetylamino)propyl]carbamoyl}methyl)(carboxymethyl)amino]ethyl}{2-[bis(carboxymethyl)amino]ethyl}amino)acetic acid

N-{[4-({[7-(N-hydroxycarbamoyl)(3S,6R,7S)-4-aza-6-(2-methylpropyl)-11-oxa-5-oxobicyclo[10.2.2]hexadeca-1⁽¹⁵⁾,12⁽¹⁶⁾,13-trien-3-yl]carbonylamino}methyl)-phenyl]methyl}-4,5-bis[2-(ethoxyethylthio)acetylamino]-pentanamide

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