benzyl 4-O-acetyl-3-O-benzyl-6-O-tert-butyldimethylsilyl-2-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(N-phthalimido)-β-D-glucopyranosyl]-α-D-mannopyranoside

Base Information

Chemical Name:benzyl 4-O-acetyl-3-O-benzyl-6-O-tert-butyldimethylsilyl-2-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(N-phthalimido)-β-D-glucopyranosyl]-α-D-mannopyranoside
CAS No.:865489-00-5
Molecular Formula:C₄₈H₅₉NO₁₆Si
Molecular Weight:934.079
Hs Code.:

benzyl 4-O-acetyl-3-O-benzyl-6-O-tert-butyldimethylsilyl-2-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(N-phthalimido)-β-D-glucopyranosyl]-α-D-mannopyranoside

Synonyms:benzyl 4-O-acetyl-3-O-benzyl-6-O-tert-butyldimethylsilyl-2-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(N-phthalimido)-β-D-glucopyranosyl]-α-D-mannopyranoside

Suppliers and Price of benzyl 4-O-acetyl-3-O-benzyl-6-O-tert-butyldimethylsilyl-2-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(N-phthalimido)-β-D-glucopyranosyl]-α-D-mannopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl 4-O-acetyl-3-O-benzyl-6-O-tert-butyldimethylsilyl-2-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(N-phthalimido)-β-D-glucopyranosyl]-α-D-mannopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl 4-O-acetyl-3-O-benzyl-6-O-tert-butyldimethylsilyl-2-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(N-phthalimido)-β-D-glucopyranosyl]-α-D-mannopyranoside

There total 5 articles about benzyl 4-O-acetyl-3-O-benzyl-6-O-tert-butyldimethylsilyl-2-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(N-phthalimido)-β-D-glucopyranosyl]-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 865488-99-9
benzyl 3-O-benzyl-6-O-tert-butyldimethylsilyl-2-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(N-phthalimido)-β-D-glucopyranosyl]-α-D-mannopyranoside

: 108-24-7
acetic anhydride

: 865489-00-5
benzyl 4-O-acetyl-3-O-benzyl-6-O-tert-butyldimethylsilyl-2-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(N-phthalimido)-β-D-glucopyranosyl]-α-D-mannopyranoside

Guidance literature:: With pyridine; at 20 ℃; for 2h;
DOI:10.1016/j.bmc.2011.05.047

Reference yield:

: 865488-98-8
benzyl 3-O-benzyl-2-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(N-phthalimido)-β-D-glucopyranosyl]-α-D-mannopyranoside

: 865489-00-5
benzyl 4-O-acetyl-3-O-benzyl-6-O-tert-butyldimethylsilyl-2-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(N-phthalimido)-β-D-glucopyranosyl]-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere

2: pyridine / 2 h / 20 °C

With pyridine; 1H-imidazole; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.05.047

Reference yield:

: 865488-82-0
benzyl 3-O-benzyl-4,6-O-benzylidiene-2-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(N-phthalimido)-β-D-glucopyranosyl]-α-D-mannopyranoside

: 865489-00-5
benzyl 4-O-acetyl-3-O-benzyl-6-O-tert-butyldimethylsilyl-2-O-[3,4,6-tri-O-acetyl-2-deoxy-2-(N-phthalimido)-β-D-glucopyranosyl]-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: water; acetic acid / 2 h / 55 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere

3: pyridine / 2 h / 20 °C

With pyridine; 1H-imidazole; water; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.05.047