phenylphosphonous acid dichloride; compound with aluminium trichloride (1:1)

Base Information

• Chemical Name: phenylphosphonous acid dichloride; compound with aluminium trichloride (1:1)
• CAS No.: 82123-74-8
• Molecular Formula: AlCl₃*C₆H₅Cl₂P
• Molecular Weight: 312.326
• Mol file: 82123-74-8.mol

Synonyms:phenylphosphonous acid dichloride; compound with aluminium trichloride (1:1)

Chemical Property of phenylphosphonous acid dichloride; compound with aluminium trichloride (1:1)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phenylphosphonous acid dichloride; compound with aluminium trichloride (1:1)

There total 1 articles about phenylphosphonous acid dichloride; compound with aluminium trichloride (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → phenylphosphonous acid dichloride; compound with aluminium trichloride (1:1) (82123-74-8)

Guidance literature:

With aluminium trichloride; phosphorus trichloride; for 3h; Heating;

Reference yield:

Tris(2-chloroethyl) phosphate (115-96-8,28205-79-0) + phenylphosphonous acid dichloride; compound with aluminium trichloride (1:1) (82123-74-8) → Dichlorophenylphosphine (644-97-3) + complex of tris-2-chloroethyl phosphate with aluminum chloride

Guidance literature:

With phosphorus trichloride; at 30 ℃; for 0.333333h; Product distribution; complexes of various arylphosphonous dichlorides with aluminum chloride;

Reference yield:

phenylphosphonous acid dichloride; compound with aluminium trichloride (1:1) (82123-74-8) → sec-butylphenylphosphinic chloride (51103-88-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 2 h / 90 °C

2: 5.6 g / PCl₅ / benzene / 0.5 h / Heating

With phosphorus pentachloride; In benzene;

upstream raw materials:

benzene

Downstream raw materials:

1,4-dimethyl-2-phenyl-2-phospha-bicyclo[2.2.1]heptane 2exo-oxide

1,4-dimethyl-2-phenyl-2-phospha-bicyclo[2.2.1]heptane 2endo-oxide

1,5-dimethyl-3-phenyl-3-phospha-bicyclo[3.1.0]hexane 3-oxide

2,2,4,4-tetramethyl-1-phenyl-phospholane 1-oxide