2-(2-(2-hydroxyethoxy)ethyl)-6-(4-(1,2,2-triphenylvinyl)phenyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione

Base Information

Chemical Name:2-(2-(2-hydroxyethoxy)ethyl)-6-(4-(1,2,2-triphenylvinyl)phenyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione
CAS No.:1391632-32-8
Molecular Formula:C₄₂H₃₃NO₄
Molecular Weight:615.728
Hs Code.:

Synonyms:2-(2-(2-hydroxyethoxy)ethyl)-6-(4-(1,2,2-triphenylvinyl)phenyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione

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Chemical Property of 2-(2-(2-hydroxyethoxy)ethyl)-6-(4-(1,2,2-triphenylvinyl)phenyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione

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Technology Process of 2-(2-(2-hydroxyethoxy)ethyl)-6-(4-(1,2,2-triphenylvinyl)phenyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione

There total 5 articles about 2-(2-(2-hydroxyethoxy)ethyl)-6-(4-(1,2,2-triphenylvinyl)phenyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.3%

: 1227040-87-0
4-(1,2,2-triphenylvinyl)phenylboronic acid

: 651768-36-4
6-bromo-2-(2-(2-hydroxyethoxy)ethyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione

: 1391632-32-8
2-(2-(2-hydroxyethoxy)ethyl)-6-(4-(1,2,2-triphenylvinyl)phenyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; In water; toluene; at 90 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c2cc33218c

Reference yield:

: C₃₂H₃₃BO₂

: 1391632-32-8
2-(2-(2-hydroxyethoxy)ethyl)-6-(4-(1,2,2-triphenylvinyl)phenyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / water / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / water; toluene / 12 h / 90 °C / Inert atmosphere

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; In water; toluene;
DOI:10.1039/c2cc33218c

Reference yield:

: 101-81-5
Diphenylmethane

: 1391632-32-8
2-(2-(2-hydroxyethoxy)ethyl)-6-(4-(1,2,2-triphenylvinyl)phenyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / toluene / Reflux; Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere

3.2: Inert atmosphere

4.1: hydrogenchloride / water / Inert atmosphere

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / water; toluene / 12 h / 90 °C / Inert atmosphere

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; water; toluene;
DOI:10.1039/c2cc33218c