{PtH(NH₃)(P(C(CH₃)3)2(C₆H₅))2}⁽¹⁺⁾*PF₆^(1-)={PtH(NH₃)(P(C(CH₃)3)2(C₆H₅))2}PF₆

Base Information

• Chemical Name: {PtH(NH₃)(P(C(CH₃)3)2(C₆H₅))2}⁽¹⁺⁾*PF₆^(1-)={PtH(NH₃)(P(C(CH₃)3)2(C₆H₅))2}PF₆
• CAS No.: 85931-08-4
• Molecular Formula: C₂₈H₅₀NP₂Pt*F₆P
• Molecular Weight: 802.703

Synonyms:{PtH(NH₃)(P(C(CH₃)3)2(C₆H₅))2}⁽¹⁺⁾*PF₆^(1-)={PtH(NH₃)(P(C(CH₃)3)2(C₆H₅))2}PF₆

Chemical Property of {PtH(NH₃)(P(C(CH₃)3)2(C₆H₅))2}⁽¹⁺⁾*PF₆^(1-)={PtH(NH₃)(P(C(CH₃)3)2(C₆H₅))2}PF₆

Chemical Property:

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Technology Process of {PtH(NH₃)(P(C(CH₃)3)2(C₆H₅))2}⁽¹⁺⁾*PF₆^(1-)={PtH(NH₃)(P(C(CH₃)3)2(C₆H₅))2}PF₆

There total 1 articles about {PtH(NH₃)(P(C(CH₃)3)2(C₆H₅))2}⁽¹⁺⁾*PF₆^(1-)={PtH(NH₃)(P(C(CH₃)3)2(C₆H₅))2}PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

ammonium hexafluorophosphate + bis(di-t-butylphenylphosphine)platinum(0) (59765-06-9) → {PtH(NH3)(P(C(CH3)3)2(C6H5))2}(1+)*PF6(1-)={PtH(NH3)(P(C(CH3)3)2(C6H5))2}PF6 (85931-08-4)

Guidance literature:

In tetrahydrofuran; stirring of starting compounds in THF under Ar at 25°C for 48 h; all operations under Ar: evapn., addn. of CH2Cl2, filtration (florisil), addn. of pentane, cooling, elem. anal.;

DOI:10.1016/S0022-328X(00)98622-4

Reference yield: 90.0%

{PtH(NH3)(P(C(CH3)3)2(C6H5))2}(1+)*PF6(1-)={PtH(NH3)(P(C(CH3)3)2(C6H5))2}PF6 (85931-08-4) → bis(di-t-butylphenylphosphine)platinum(0) (59765-06-9)

Guidance literature:

With ammonia; In acetone; under Ar; bubbling of NH3 through an acetone solution of teh Pt complex at 25°C; filtration, washing with acetone, drying, NMR anal.;

DOI:10.1016/S0022-328X(00)98622-4

Reference yield:

{PtH(NH3)(P(C(CH3)3)2(C6H5))2}(1+)*PF6(1-)={PtH(NH3)(P(C(CH3)3)2(C6H5))2}PF6 (85931-08-4) → {PtH(CO)(P(C(CH3)3)2(C6H5))2}(1+)*PF6(1-)={PtH(CO)(P(C(CH3)3)2(C6H5))2}PF6 (85931-10-8)

Guidance literature:

With carbon monoxide; In dichloromethane; byproducts: NH3; CO bubbled into a CH2Cl2 solution of the Pt complex at 25°C; all operations under Ar: filtration, washing with acetone, elem. anal.;

DOI:10.1016/S0022-328X(00)98622-4

upstream raw materials:

bis(di-t-butylphenylphosphine)platinum⁽⁰⁾

Downstream raw materials:

bis(di-t-butylphenylphosphine)platinum⁽⁰⁾

{PtH(CO)(P(C(CH₃)3)2(C₆H₅))2}⁽¹⁺⁾*PF₆^(1-)={PtH(CO)(P(C(CH₃)3)2(C₆H₅))2}PF₆

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