orcinolbis(diphenyl)phosphinite

Base Information

• Chemical Name: orcinolbis(diphenyl)phosphinite
• CAS No.: 315667-10-8
• Molecular Formula: C₃₁H₂₆O₂P₂
• Molecular Weight: 492.494
• Mol file: 315667-10-8.mol

Synonyms:orcinolbis(diphenyl)phosphinite

Chemical Property of orcinolbis(diphenyl)phosphinite

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of orcinolbis(diphenyl)phosphinite

There total 1 articles about orcinolbis(diphenyl)phosphinite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

orcinol (504-15-4) + chloro-diphenylphosphine (1079-66-9,74391-44-9) → orcinolbis(diphenyl)phosphinite (315667-10-8)

Guidance literature:

With triethylamine; In toluene; heating;

DOI:10.1039/b004793g

Reference yield: 78.0%

palladium(II) trifluoroacetate + orcinolbis(diphenyl)phosphinite (315667-10-8) → Pd(CH((C(OP(C6H5)2)CH)2CCH3))(OC(O)CF3) (315667-12-0)

Guidance literature:

In tetrahydrofuran; under N2; soln. of Pd(OCOCF3)2 and orcinolbis(diphenyl)phosphinite (1:1 mol) in THF stirred at room temp. 2 h; evapd. (vac.); residue washed (EtOH); crystd. (CH2Cl2-EtOH); elem. anal.;

DOI:10.1039/b004793g

upstream raw materials:

orcinol

chloro-diphenylphosphine

Downstream raw materials:

Pd(CH((C(OP(C₆H₅)2)CH)2CCH₃))(OC(O)CF₃)