N-hydroxy(2-phenylethyl)-oximidoyl chloride

Base Information

Chemical Name:N-hydroxy(2-phenylethyl)-oximidoyl chloride
CAS No.:92988-96-0
Molecular Formula:C₉H₁₀ClNO
Molecular Weight:183.637
Hs Code.:

Synonyms:N-hydroxy(2-phenylethyl)-oximidoyl chloride

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Chemical Property of N-hydroxy(2-phenylethyl)-oximidoyl chloride

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Technology Process of N-hydroxy(2-phenylethyl)-oximidoyl chloride

There total 3 articles about N-hydroxy(2-phenylethyl)-oximidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1197-50-8
3-phenylpropanal oxime

: 92988-96-0
N-hydroxy(2-phenylethyl)-oximidoyl chloride

Guidance literature:: With N-chloro-succinimide; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1016/j.tet.2009.04.043

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 92988-96-0
N-hydroxy(2-phenylethyl)-oximidoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; pyridine / methanol / 2.5 h / 20 °C

2: N-chloro-succinimide / N,N-dimethyl-formamide / 35 °C / Cooling with ice

With pyridine; N-chloro-succinimide; hydroxylamine hydrochloride; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2013.07.049

Reference yield:

: 122-97-4
3-Phenyl-1-propanol

: 92988-96-0
N-hydroxy(2-phenylethyl)-oximidoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: [bis(acetoxy)iodo]benzene; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 3 h / 20 °C / Inert atmosphere

2: hydroxylamine hydrochloride; potassium carbonate / dichloromethane / 18 h / 20 °C / Inert atmosphere

3: N-chloro-succinimide / dichloromethane; N,N-dimethyl-formamide / 4 h / 0 - 20 °C / Inert atmosphere

With N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; hydroxylamine hydrochloride; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-0039-1690102