N₁-[4-(3,5-bistrifluoro-methylpyrazol-1-ylmethyl)-2-methylphenyl]-N₂-(1,1-dimethyl-2-methylsulfanylethyl)-3-iodophthalamide

Base Information

• Chemical Name: N₁-[4-(3,5-bistrifluoro-methylpyrazol-1-ylmethyl)-2-methylphenyl]-N₂-(1,1-dimethyl-2-methylsulfanylethyl)-3-iodophthalamide
• CAS No.: 866635-96-3
• Molecular Formula: C₂₆H₂₅F₆IN₄O₂S
• Molecular Weight: 698.471

Synonyms:N₁-[4-(3,5-bistrifluoro-methylpyrazol-1-ylmethyl)-2-methylphenyl]-N₂-(1,1-dimethyl-2-methylsulfanylethyl)-3-iodophthalamide

Chemical Property of N₁-[4-(3,5-bistrifluoro-methylpyrazol-1-ylmethyl)-2-methylphenyl]-N₂-(1,1-dimethyl-2-methylsulfanylethyl)-3-iodophthalamide

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Technology Process of N₁-[4-(3,5-bistrifluoro-methylpyrazol-1-ylmethyl)-2-methylphenyl]-N₂-(1,1-dimethyl-2-methylsulfanylethyl)-3-iodophthalamide

There total 2 articles about N₁-[4-(3,5-bistrifluoro-methylpyrazol-1-ylmethyl)-2-methylphenyl]-N₂-(1,1-dimethyl-2-methylsulfanylethyl)-3-iodophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(1,1-dimethyl-2-methylthioethylimino)-4-iodo-3H-isobenzofuran-1-one + 4-{[3,5-bis(trifluoro-methyl)-1H-pyrazol-1-yl]methyl}-2-methylaniline (866638-67-7) → N1-[4-(3,5-bistrifluoro-methylpyrazol-1-ylmethyl)-2-methylphenyl]-N2-(1,1-dimethyl-2-methylsulfanylethyl)-3-iodophthalamide (866635-96-3)

Guidance literature:

With toluene-4-sulfonic acid; In acetonitrile; at 60 ℃; for 3h;

Reference yield:

→ N1-[4-(3,5-bistrifluoro-methylpyrazol-1-ylmethyl)-2-methylphenyl]-N2-(1,1-dimethyl-2-methylsulfanylethyl)-3-iodophthalamide (866635-96-3)

Guidance literature:

Reference yield:

N1-[4-(3,5-bistrifluoro-methylpyrazol-1-ylmethyl)-2-methylphenyl]-N2-(1,1-dimethyl-2-methylsulfanylethyl)-3-iodophthalamide (866635-96-3) → N1-{4-[3,5-bis(trifluoromethyl)-1H-pyrazol-1-ylmethyl]-2-methylphenyl}-3-iodo-N2-(2-methanesulfonyl-1,1-dimethylethyl)phthalamide (866635-98-5)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 5h;

upstream raw materials:

4-{[3,5-bis(trifluoro-methyl)-1H-pyrazol-1-yl]methyl}-2-methylaniline

Downstream raw materials:

N₁-{4-[3,5-bis(trifluoromethyl)-1H-pyrazol-1-ylmethyl]-2-methylphenyl}-3-iodo-N₂-(2-methanesulfonyl-1,1-dimethylethyl)phthalamide

N₁-{4-[3,5-bis(trifluoromethyl)-1H-pyrazol-1-ylmethyl]-2-methylphenyl}-N₂-(2-methanesulfinyl-1,1-dimethylethyl)-3-iodophthalamide

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