C₂₃H₂₈F₃NO₅S

Base Information

Chemical Name:C₂₃H₂₈F₃NO₅S
CAS No.:1253217-03-6
Molecular Formula:C₂₃H₂₈F₃NO₅S
Molecular Weight:487.54
Hs Code.:

C<sub>23</sub>H<sub>28</sub>F<sub>3</sub>NO<sub>5</sub>S

Synonyms:C₂₃H₂₈F₃NO₅S

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Chemical Property of C₂₃H₂₈F₃NO₅S

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Technology Process of C₂₃H₂₈F₃NO₅S

There total 9 articles about C₂₃H₂₈F₃NO₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1253214-98-0
C₂₂H₂₉NO₃

: 1253217-03-6
C₂₃H₂₈F₃NO₅S

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; Cooling with ice;

Reference yield:

: 939430-71-4
6-chloro-5-methoxymethoxy-pyridine-2-carbaldehyde

: 1253217-03-6
C₂₃H₂₈F₃NO₅S

Guidance literature:: Multi-step reaction with 8 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 2.83 h / -78 - 20 °C

2.1: acetic acid / ethanol / 7 h / 50 °C

3.1: caesium carbonate / tetrahydrofuran; acetonitrile / 4 h

4.1: pyridine / 18 h

5.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 0.17 h / 0 °C / Cooling with ice

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / 1,2-dimethoxyethane; water / 24 h / 90 °C / Inert atmosphere

7.1: palladium 10% on activated carbon; hydrogen / ethanol / 9 h / Inert atmosphere

8.1: N-ethyl-N,N-diisopropylamine / dichloromethane / Cooling with ice

With pyridine; triethylsilane; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; palladium 10% on activated carbon; boron trifluoride diethyl etherate; hydrogen; caesium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; hexane; dichloromethane; water; acetonitrile;

Reference yield:

: 848442-41-1
C₁₂H₁₇BrO₂

: 1253217-03-6
C₂₃H₂₈F₃NO₅S

Guidance literature:: Multi-step reaction with 8 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 2.83 h / -78 - 20 °C

2.1: acetic acid / ethanol / 7 h / 50 °C

3.1: caesium carbonate / tetrahydrofuran; acetonitrile / 4 h

4.1: pyridine / 18 h

5.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 0.17 h / 0 °C / Cooling with ice

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / 1,2-dimethoxyethane; water / 24 h / 90 °C / Inert atmosphere

7.1: palladium 10% on activated carbon; hydrogen / ethanol / 9 h / Inert atmosphere

8.1: N-ethyl-N,N-diisopropylamine / dichloromethane / Cooling with ice

With pyridine; triethylsilane; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; palladium 10% on activated carbon; boron trifluoride diethyl etherate; hydrogen; caesium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; hexane; dichloromethane; water; acetonitrile;