2,6-dimethoxy-1-O-(3'-carbomethoxypropyl)-4-O-triisopropylsilyl-1,4-hydroquinone

Base Information

Chemical Name:2,6-dimethoxy-1-O-(3'-carbomethoxypropyl)-4-O-triisopropylsilyl-1,4-hydroquinone
CAS No.:205868-68-4
Molecular Formula:C₂₂H₃₈O₆Si
Molecular Weight:426.626
Hs Code.:

Synonyms:2,6-dimethoxy-1-O-(3'-carbomethoxypropyl)-4-O-triisopropylsilyl-1,4-hydroquinone

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Chemical Property of 2,6-dimethoxy-1-O-(3'-carbomethoxypropyl)-4-O-triisopropylsilyl-1,4-hydroquinone

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Technology Process of 2,6-dimethoxy-1-O-(3'-carbomethoxypropyl)-4-O-triisopropylsilyl-1,4-hydroquinone

There total 7 articles about 2,6-dimethoxy-1-O-(3'-carbomethoxypropyl)-4-O-triisopropylsilyl-1,4-hydroquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 4897-84-1
Methyl 4-bromobutyrate

: 205868-66-2
2,6-dimethoxy-4-O-triisopropylsilyl-1,4-hydroquinone

: 205868-68-4
2,6-dimethoxy-1-O-(3'-carbomethoxypropyl)-4-O-triisopropylsilyl-1,4-hydroquinone

Guidance literature:: With 18-crown-6 ether; potassium carbonate; potassium iodide; In acetonitrile; for 14h; Heating;

Reference yield:

: 13154-24-0
triisopropylsilyl chloride

: 205868-68-4
2,6-dimethoxy-1-O-(3'-carbomethoxypropyl)-4-O-triisopropylsilyl-1,4-hydroquinone

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole / 1.) DMF, 30 min, 2.) DMF, 3 d

2: 86 percent / Amberlite IRA 420(OH) resin / methanol / 48 h

3: K₂CO₃ / 1.) butanone, 1 h, 2.) butanone, reflux, 3 d

With 1H-imidazole; Amberlite IRA 420(OH) resin; potassium carbonate; In methanol;

Reference yield:

: 134778-17-9
(3,5-dimethoxyphenoxy)triisopropylsilane

: 205868-68-4
2,6-dimethoxy-1-O-(3'-carbomethoxypropyl)-4-O-triisopropylsilyl-1,4-hydroquinone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi, 2.) triisopropyl borate, 3.) aq. H₂O₂, aq. NaOH

2: K₂CO₃ / 1.) butanone, 1 h, 2.) butanone, reflux, 3 d

With sodium hydroxide; n-butyllithium; Triisopropyl borate; dihydrogen peroxide; potassium carbonate;