(3-Amino-2,2'-dioxo-4,4'-diphenyl-[1,3']biazetidinyl-1'-yl)-acetic acid tert-butyl ester

Base Information

Chemical Name:(3-Amino-2,2'-dioxo-4,4'-diphenyl-[1,3']biazetidinyl-1'-yl)-acetic acid tert-butyl ester
CAS No.:78043-79-5
Molecular Formula:C₂₄H₂₇N₃O₄
Molecular Weight:421.496
Hs Code.:

Synonyms:(3-Amino-2,2'-dioxo-4,4'-diphenyl-[1,3']biazetidinyl-1'-yl)-acetic acid tert-butyl ester

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Chemical Property of (3-Amino-2,2'-dioxo-4,4'-diphenyl-[1,3']biazetidinyl-1'-yl)-acetic acid tert-butyl ester

Chemical Property:

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Technology Process of (3-Amino-2,2'-dioxo-4,4'-diphenyl-[1,3']biazetidinyl-1'-yl)-acetic acid tert-butyl ester

There total 5 articles about (3-Amino-2,2'-dioxo-4,4'-diphenyl-[1,3']biazetidinyl-1'-yl)-acetic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: (3-Azido-2,2'-dioxo-4,4'-diphenyl-[1,3']biazetidinyl-1'-yl)-acetic acid tert-butyl ester

: 78043-79-5
(3-Amino-2,2'-dioxo-4,4'-diphenyl-[1,3']biazetidinyl-1'-yl)-acetic acid tert-butyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; ethyl acetate; at 50 ℃; under 760 Torr;
DOI:10.1246/cl.1981.231

Reference yield:

: 64923-12-2
tert-butyl N-benzylideneglycinate

: 78043-79-5
(3-Amino-2,2'-dioxo-4,4'-diphenyl-[1,3']biazetidinyl-1'-yl)-acetic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 56 percent / triethylamine / CH₂Cl₂

2: 90 percent / H₂ / 5percent Pd-C / methanol / 760 Torr / Ambient temperature

3: 100 percent / sodium sulfate / benzene

4: 58 percent / triethylamine / CH₂Cl₂

5: 99 percent / H₂ / 10 percent Pd-C / ethyl acetate; ethanol / 50 °C / 760 Torr

With hydrogen; sodium sulfate; triethylamine; palladium on activated charcoal; In methanol; ethanol; dichloromethane; ethyl acetate; benzene;
DOI:10.1246/cl.1981.231

Reference yield:

: 78029-07-9
(3-Amino-2-oxo-4-phenyl-azetidin-1-yl)-acetic acid tert-butyl ester

: 78043-79-5
(3-Amino-2,2'-dioxo-4,4'-diphenyl-[1,3']biazetidinyl-1'-yl)-acetic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / sodium sulfate / benzene

2: 58 percent / triethylamine / CH₂Cl₂

3: 99 percent / H₂ / 10 percent Pd-C / ethyl acetate; ethanol / 50 °C / 760 Torr

With hydrogen; sodium sulfate; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; ethyl acetate; benzene;
DOI:10.1246/cl.1981.231