Technology Process of C50H84N6O8
There total 2 articles about C50H84N6O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C51H86N6O8;
With
lithium hydroxide;
In
tetrahydrofuran; water; tert-butyl alcohol;
at 20 ℃;
Inert atmosphere;
With
hydrogenchloride;
In
water;
pH=1;
Inert atmosphere;
DOI:10.1021/np300834q
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / -78 °C / Inert atmosphere
1.2: 4 h / -78 - 20 °C / Inert atmosphere
2.1: lithium hydroxide / tetrahydrofuran; tert-butyl alcohol; water / 20 °C / Inert atmosphere
2.2: pH 1 / Inert atmosphere
With
sodium hydride; lithium hydroxide;
In
tetrahydrofuran; water; mineral oil; tert-butyl alcohol;
DOI:10.1021/np300834q
- Guidance literature:
-
C50H84N6O8;
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
for 0.333333h;
Inert atmosphere;
N-(3-phenylpropionyl)-1,2-ethanediamine;
In
dichloromethane;
at 20 ℃;
for 12h;
Inert atmosphere;
DOI:10.1021/np300834q