3,4-di-O-acetyl-2-deoxy-2-(p-methoxybenzylideneamino)-6-O-tosyl-α-D-glucopyranosyl bromide

Base Information

Chemical Name:3,4-di-O-acetyl-2-deoxy-2-(p-methoxybenzylideneamino)-6-O-tosyl-α-D-glucopyranosyl bromide
CAS No.:63064-79-9
Molecular Formula:C₂₅H₂₈BrNO₉S
Molecular Weight:598.469
Hs Code.:

Synonyms:3,4-di-O-acetyl-2-deoxy-2-(p-methoxybenzylideneamino)-6-O-tosyl-α-D-glucopyranosyl bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-di-O-acetyl-2-deoxy-2-(p-methoxybenzylideneamino)-6-O-tosyl-α-D-glucopyranosyl bromide

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Technology Process of 3,4-di-O-acetyl-2-deoxy-2-(p-methoxybenzylideneamino)-6-O-tosyl-α-D-glucopyranosyl bromide

There total 1 articles about 3,4-di-O-acetyl-2-deoxy-2-(p-methoxybenzylideneamino)-6-O-tosyl-α-D-glucopyranosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 6619-11-0
1,3,4-tri-O-acetyl-2-deoxy-2-(p-methoxybenzylideneamino)-6-O-tosyl-β-D-glucopyranose

: 63064-79-9
3,4-di-O-acetyl-2-deoxy-2-(p-methoxybenzylideneamino)-6-O-tosyl-α-D-glucopyranosyl bromide

Guidance literature:: With hydrogen bromide; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1246/bcsj.53.3259

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 63064-79-9
3,4-di-O-acetyl-2-deoxy-2-(p-methoxybenzylideneamino)-6-O-tosyl-α-D-glucopyranosyl bromide

: 63064-76-6
6,3',4',5-tetra-O-acetyl-1,3,2',6'-tetra-N-(benzyloxycarbonyl)ribostamycin

: 63064-77-7
6,3',4',5,3''',4'''-hexa-O-acetyl-1,3,2',6',2'''-penta-N-(benzyloxycarbonyl)-6'''-deamino-6'''-tosyloxyneomycin C

Guidance literature:: With hydrogenchloride; calcium sulfate; silver perchlorate; sodium carbonate; silver carbonate; Yield given. Multistep reaction;
DOI:10.1246/bcsj.53.3259