N-alloc-O-PMB vancomycin aglycon allyl ester

Base Information

Chemical Name:N-alloc-O-PMB vancomycin aglycon allyl ester
CAS No.:220971-89-1
Molecular Formula:C₆₈H₆₈Cl₂N₈O₂₀
Molecular Weight:1388.24
Hs Code.:

Synonyms:N-alloc-O-PMB vancomycin aglycon allyl ester

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Chemical Property of N-alloc-O-PMB vancomycin aglycon allyl ester

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Technology Process of N-alloc-O-PMB vancomycin aglycon allyl ester

There total 3 articles about N-alloc-O-PMB vancomycin aglycon allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 824-94-2
p-methoxybenzyl chloride

: 220971-99-3
N-alloc vancomycin aglycon allyl ester

: 220971-89-1
N-alloc-O-PMB vancomycin aglycon allyl ester

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; for 2h;
DOI:10.1021/ja983504u

Reference yield:

: 82198-76-3
vancomycin aglycon

: 220971-89-1
N-alloc-O-PMB vancomycin aglycon allyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: aq. NaHCO₃ / dioxane / 3 h / Ambient temperature

2: KHCO₃ / 1.) DMF, 30 min, 2.) DMF, 3 h

3: 71 percent / Cs₂CO₃ / dimethylformamide / 2 h

With sodium hydrogencarbonate; potassium hydrogencarbonate; caesium carbonate; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1021/ja983504u

Reference yield:

: 220971-98-2
N-alloc vancomycin aglycon

: 220971-89-1
N-alloc-O-PMB vancomycin aglycon allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: KHCO₃ / 1.) DMF, 30 min, 2.) DMF, 3 h

2: 71 percent / Cs₂CO₃ / dimethylformamide / 2 h

With potassium hydrogencarbonate; caesium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/ja983504u