2-[2-(4-{2-Hydroxy-5-[2-(3-methoxy-phenyl)-ethyl]-phenoxy}-phenyl)-ethyl]-[1,4]benzoquinone

Base Information

Chemical Name:2-[2-(4-{2-Hydroxy-5-[2-(3-methoxy-phenyl)-ethyl]-phenoxy}-phenyl)-ethyl]-[1,4]benzoquinone
CAS No.:135203-63-3
Molecular Formula:C₂₉H₂₆O₅
Molecular Weight:454.522
Hs Code.:

Synonyms:2-[2-(4-{2-Hydroxy-5-[2-(3-methoxy-phenyl)-ethyl]-phenoxy}-phenyl)-ethyl]-[1,4]benzoquinone

Suppliers and Price of 2-[2-(4-{2-Hydroxy-5-[2-(3-methoxy-phenyl)-ethyl]-phenoxy}-phenyl)-ethyl]-[1,4]benzoquinone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-[2-(4-{2-Hydroxy-5-[2-(3-methoxy-phenyl)-ethyl]-phenoxy}-phenyl)-ethyl]-[1,4]benzoquinone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-[2-(4-{2-Hydroxy-5-[2-(3-methoxy-phenyl)-ethyl]-phenoxy}-phenyl)-ethyl]-[1,4]benzoquinone

There total 9 articles about 2-[2-(4-{2-Hydroxy-5-[2-(3-methoxy-phenyl)-ethyl]-phenoxy}-phenyl)-ethyl]-[1,4]benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.4%

: 135203-65-5
C₅₀H₄₂O₅

: 135203-63-3
2-[2-(4-{2-Hydroxy-5-[2-(3-methoxy-phenyl)-ethyl]-phenoxy}-phenyl)-ethyl]-[1,4]benzoquinone

: 135203-47-3
14-hydroxyperottetin E-11'-methyl ether

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; Ambient temperature;
DOI:10.1016/0031-9422(91)84201-3

Reference yield: 50.2%

: 135203-47-3
14-hydroxyperottetin E-11'-methyl ether

: 135203-63-3
2-[2-(4-{2-Hydroxy-5-[2-(3-methoxy-phenyl)-ethyl]-phenoxy}-phenyl)-ethyl]-[1,4]benzoquinone

Guidance literature:: In chloroform; for 120h; Ambient temperature;
DOI:10.1016/0031-9422(91)84201-3

Reference yield:

: 5798-75-4
Ethyl 4-bromobenzoate

: 135203-63-3
2-[2-(4-{2-Hydroxy-5-[2-(3-methoxy-phenyl)-ethyl]-phenoxy}-phenyl)-ethyl]-[1,4]benzoquinone

Guidance literature:: Multi-step reaction with 6 steps

1: 81.3 percent / K₂CO₃, CuO / pyridine / 24 h / Heating

2: 1) KOt-Bu / 1) DMF, 0-5 deg C, 15 min, 2) DMF, 4h, r. t.

3: 99.1 percent / LiAlH₄ / diethyl ether / 4 h / Ambient temperature

4: 95.1 percent / pyridinium dichromate / CH₂Cl₂ / 12 h

5: 1) KOt-Bu / 1) DMF, 0-5 deg C, 15 min, 2) DMF, r. t.

6: 13.8 percent / H₂ / 20percent Pd-C / ethyl acetate / Ambient temperature

With lithium aluminium tetrahydride; dipyridinium dichromate; potassium tert-butylate; hydrogen; potassium carbonate; copper(II) oxide; palladium on activated charcoal; In pyridine; diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1016/0031-9422(91)84201-3