diethyl S-benzohydroximinoylthiomethylphosphonate

Base Information

Chemical Name:diethyl S-benzohydroximinoylthiomethylphosphonate
CAS No.:900816-60-6
Molecular Formula:C₁₂H₁₈NO₄PS
Molecular Weight:303.319
Hs Code.:

Synonyms:diethyl S-benzohydroximinoylthiomethylphosphonate

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Chemical Property of diethyl S-benzohydroximinoylthiomethylphosphonate

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Technology Process of diethyl S-benzohydroximinoylthiomethylphosphonate

There total 1 articles about diethyl S-benzohydroximinoylthiomethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 70660-08-1
S-(diethoxyphosphoryl)methyl ethanethioate

: 698-16-8
benzohydroximoyl chloride

: 900816-60-6
diethyl S-benzohydroximinoylthiomethylphosphonate

Guidance literature:: S-(diethoxyphosphoryl)methyl ethanethioate; With sodium methylate; In ethanol; at 20 ℃; for 2h;

benzohydroximoyl chloride; With triethylamine; In tetrahydrofuran; ethanol; at 20 ℃;
DOI:10.1071/CH05190

Reference yield: 67.0%

: 900816-60-6
diethyl S-benzohydroximinoylthiomethylphosphonate

: 2-ethoxy-5-phenyl-1,2,3,4-tetrahydro-1,4,6,2-oxathiazaphosphorine 2-oxide

Guidance literature:: With sodium hydroxide; In benzene; for 2h; Heating;
DOI:10.1071/CH05190

Reference yield:

: 900816-60-6
diethyl S-benzohydroximinoylthiomethylphosphonate

: ethyl methyl S-benzohydroximinoylthiomethylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / sodium hydroxide / benzene / 2 h / Heating

2: 2 mg / 18 h / 60 °C

With sodium hydroxide; In benzene;
DOI:10.1071/CH05190