diethyl S-benzohydroximinoylthiomethylphosphonate

Base Information

• Chemical Name: diethyl S-benzohydroximinoylthiomethylphosphonate
• CAS No.: 900816-60-6
• Molecular Formula: C₁₂H₁₈NO₄PS
• Molecular Weight: 303.319
• Mol file: 900816-60-6.mol

Synonyms:diethyl S-benzohydroximinoylthiomethylphosphonate

Chemical Property of diethyl S-benzohydroximinoylthiomethylphosphonate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of diethyl S-benzohydroximinoylthiomethylphosphonate

There total 1 articles about diethyl S-benzohydroximinoylthiomethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

S-(diethoxyphosphoryl)methyl ethanethioate (70660-08-1) + benzohydroximoyl chloride (698-16-8) → diethyl S-benzohydroximinoylthiomethylphosphonate (900816-60-6)

Guidance literature:

S-(diethoxyphosphoryl)methyl ethanethioate; With sodium methylate; In ethanol; at 20 ℃; for 2h;

benzohydroximoyl chloride; With triethylamine; In tetrahydrofuran; ethanol; at 20 ℃;

DOI:10.1071/CH05190

Reference yield: 67.0%

diethyl S-benzohydroximinoylthiomethylphosphonate (900816-60-6) → 2-ethoxy-5-phenyl-1,2,3,4-tetrahydro-1,4,6,2-oxathiazaphosphorine 2-oxide

Guidance literature:

With sodium hydroxide; In benzene; for 2h; Heating;

DOI:10.1071/CH05190

Reference yield:

diethyl S-benzohydroximinoylthiomethylphosphonate (900816-60-6) → ethyl methyl S-benzohydroximinoylthiomethylphosphonate

Guidance literature:

Multi-step reaction with 2 steps

1: 67 percent / sodium hydroxide / benzene / 2 h / Heating

2: 2 mg / 18 h / 60 °C

With sodium hydroxide; In benzene;

DOI:10.1071/CH05190

upstream raw materials:

S-(diethoxyphosphoryl)methyl ethanethioate

benzohydroximoyl chloride