(S)-5-((2R,4S,5R)-5-Hydroxy-2-phenyl-[1,3]dioxan-4-yl)-4-methyl-pentanal

Base Information

Chemical Name:(S)-5-((2R,4S,5R)-5-Hydroxy-2-phenyl-[1,3]dioxan-4-yl)-4-methyl-pentanal
CAS No.:669005-41-8
Molecular Formula:C₁₆H₂₂O₄
Molecular Weight:278.348
Hs Code.:

Synonyms:(S)-5-((2R,4S,5R)-5-Hydroxy-2-phenyl-[1,3]dioxan-4-yl)-4-methyl-pentanal

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Chemical Property of (S)-5-((2R,4S,5R)-5-Hydroxy-2-phenyl-[1,3]dioxan-4-yl)-4-methyl-pentanal

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Technology Process of (S)-5-((2R,4S,5R)-5-Hydroxy-2-phenyl-[1,3]dioxan-4-yl)-4-methyl-pentanal

There total 4 articles about (S)-5-((2R,4S,5R)-5-Hydroxy-2-phenyl-[1,3]dioxan-4-yl)-4-methyl-pentanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 342901-77-3
(2R,4S,5R)-4-((S)-2,6-Dimethyl-hept-5-enyl)-2-phenyl-[1,3]dioxan-5-ol

: 669005-41-8
(S)-5-((2R,4S,5R)-5-Hydroxy-2-phenyl-[1,3]dioxan-4-yl)-4-methyl-pentanal

Guidance literature:: (2R,4S,5R)-4-((S)-2,6-Dimethyl-hept-5-enyl)-2-phenyl-[1,3]dioxan-5-ol; With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; acetone; at 20 ℃;

With sodium periodate; In water; acetone;
DOI:10.1002/1521-3773(20010316)40:6<1090::AID-ANIE10900>3.0.CO;2-W

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 669005-41-8
(S)-5-((2R,4S,5R)-5-Hydroxy-2-phenyl-[1,3]dioxan-4-yl)-4-methyl-pentanal

Guidance literature:: Multi-step reaction with 2 steps

1.1: 61 percent / camphorsulfonic acid / CH₂Cl₂ / 20 °C

2.1: OsO₄; N-methylmorpholine N-oxide / acetone; H₂O / 20 °C

2.2: 70 percent / NaIO₄ / acetone; H₂O

With osmium(VIII) oxide; camphor-10-sulfonic acid; 4-methylmorpholine N-oxide; In dichloromethane; water; acetone;
DOI:10.1002/1521-3773(20010316)40:6<1090::AID-ANIE10900>3.0.CO;2-W

Reference yield:

: 669005-16-7
(2R,3S,5S)-5,9-Dimethyl-dec-8-ene-1,2,3-triol

: 669005-41-8
(S)-5-((2R,4S,5R)-5-Hydroxy-2-phenyl-[1,3]dioxan-4-yl)-4-methyl-pentanal

Guidance literature:: Multi-step reaction with 2 steps

1.1: 61 percent / camphorsulfonic acid / CH₂Cl₂ / 20 °C

2.1: OsO₄; N-methylmorpholine N-oxide / acetone; H₂O / 20 °C

2.2: 70 percent / NaIO₄ / acetone; H₂O

With osmium(VIII) oxide; camphor-10-sulfonic acid; 4-methylmorpholine N-oxide; In dichloromethane; water; acetone;
DOI:10.1002/1521-3773(20010316)40:6<1090::AID-ANIE10900>3.0.CO;2-W