ferrocenylcarbaldehyde hydrazone

Base Information

• Chemical Name: ferrocenylcarbaldehyde hydrazone
• CAS No.: 112397-39-4
• Molecular Formula: C₁₁H₁₂FeN₂
• Molecular Weight: 228.077

Synonyms:ferrocenylcarbaldehyde hydrazone

Chemical Property of ferrocenylcarbaldehyde hydrazone

Chemical Property:

Purity/Quality:

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Technology Process of ferrocenylcarbaldehyde hydrazone

There total 1 articles about ferrocenylcarbaldehyde hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

ferrocenecarboxaldehyde (12093-10-6) + C11H15N2O4S(1-)*Na(1+) → ferrocenylcarbaldehyde hydrazone (112397-39-4) + C22H23FeN2O4S(1-)*Na(1+)

Guidance literature:

In methanol; at 45 ℃; for 24h;

DOI:10.1016/j.jorganchem.2015.04.029

Reference yield: 53.0%

ferrocenylcarbaldehyde hydrazone (112397-39-4) + 2-bromo-4-phenylbutane (143097-80-7,21953-83-3) → 1-(2-methyl-4-phenylbutyl)ferrocene

Guidance literature:

With 1,1'-bis-(diphenylphosphino)ferrocene; bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; sodium t-butanolate; In tetrahydrofuran; at 80 ℃; for 12h; Inert atmosphere; Sealed tube;

DOI:10.1039/c9cc00307j

Reference yield:

ferrocenylcarbaldehyde hydrazone (112397-39-4) + buta-1,3-dien-1-ylbenzene (1515-78-2) → C21H22Fe

Guidance literature:

With [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; 1,2-bis(dimethylphosphanyl)ethane; lithium tert-butoxide; In tetrahydrofuran; at 80 ℃; for 12h; regioselective reaction; Sealed tube; Inert atmosphere;

DOI:10.1002/anie.201915875

upstream raw materials:

ferrocenecarboxaldehyde

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