(2S)-3-<<(4-methoxyphenyl)diphenylmethyl>oxy>-1,2-propylene trithiocarbonate

Base Information

Chemical Name:(2S)-3-<<(4-methoxyphenyl)diphenylmethyl>oxy>-1,2-propylene trithiocarbonate
CAS No.:161391-91-9
Molecular Formula:C₂₄H₂₂O₂S₃
Molecular Weight:438.635
Hs Code.:

Synonyms:(2S)-3-<<(4-methoxyphenyl)diphenylmethyl>oxy>-1,2-propylene trithiocarbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S)-3-<<(4-methoxyphenyl)diphenylmethyl>oxy>-1,2-propylene trithiocarbonate

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Technology Process of (2S)-3-<<(4-methoxyphenyl)diphenylmethyl>oxy>-1,2-propylene trithiocarbonate

There total 1 articles about (2S)-3-<<(4-methoxyphenyl)diphenylmethyl>oxy>-1,2-propylene trithiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 75-15-0,12122-00-8
carbon disulfide

: (S)-2-[(4-Methoxy-phenyl)-diphenyl-methoxymethyl]-oxirane

: 161391-91-9
(2S)-3-<<(4-methoxyphenyl)diphenylmethyl>oxy>-1,2-propylene trithiocarbonate

Guidance literature:: With potassium hydroxide; In methanol; for 2h; Heating;
DOI:10.1021/jm00050a009

Reference yield:

: 161391-91-9
(2S)-3-<<(4-methoxyphenyl)diphenylmethyl>oxy>-1,2-propylene trithiocarbonate

: 1026357-44-7
(S)-3-[(4-Methoxy-phenyl)-diphenyl-methoxy]-propane-1,2-dithiol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; at 25 ℃; for 1h;
DOI:10.1021/jm00050a009

Reference yield:

: 161391-91-9
(2S)-3-<<(4-methoxyphenyl)diphenylmethyl>oxy>-1,2-propylene trithiocarbonate

: 1027902-07-3
Octanethioic acid S-{(S)-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-1-octanoylsulfanylmethyl-ethyl} ester

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether; tetrahydrofuran / 1 h / 25 °C

2: pyridine / hexane / 14 h / 25 °C

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1021/jm00050a009