aceanthrenecyclone

Base Information

Chemical Name:aceanthrenecyclone
CAS No.:859818-69-2
Molecular Formula:C₃₁H₁₈O
Molecular Weight:406.483
Hs Code.:

Synonyms:aceanthrenecyclone

Suppliers and Price of aceanthrenecyclone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of aceanthrenecyclone

Chemical Property:

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Technology Process of aceanthrenecyclone

There total 1 articles about aceanthrenecyclone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6373-11-1
aceanthrenequinone

: 102-04-5
1,3-Diphenylpropanone

: 859818-69-2
aceanthrenecyclone

Guidance literature:: With methanol; sodium methylate;

Reference yield: 47.0%

: 7719-09-7
thionyl chloride

: 859818-69-2
aceanthrenecyclone

: 110-46-3
isopentyl nitrite

: C₃₃H₁₉Cl₂NO₃

: 1-chloro-1,3-diphenyl-1H-cyclopenta[a]aceanthrylene-2,7-dione

Guidance literature:: aceanthrenecyclone; isopentyl nitrite; With 3-aminophthalic acid; In dichloromethane; for 2.76667h; Reflux;

thionyl chloride; In toluene; Reflux;
DOI:10.1016/j.tet.2015.01.051

Reference yield:

: 859818-69-2
aceanthrenecyclone

: (+)-1-chloro-1,3-diphenyl-1H-cyclopenta[a]aceanthrylene-2,7-dione

: (-)-1-chloro-1,3-diphenyl-1H-cyclopenta[a]aceanthrylene-2,7-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3-aminophthalic acid / dichloromethane / 2.77 h / Reflux

1.2: Reflux

2.1: preparative SFC on a 2cm×25cm Chiralcel OZ-H column eluted with 30percent isopropanol in CO₂ / isopropyl alcohol / 75007.5 Torr / Resolution of racemate

With 3-aminophthalic acid; In dichloromethane; isopropyl alcohol;
DOI:10.1016/j.tet.2015.01.051