ethyl 2-O-4-(2-(dimethylsilyloxy)ethyl)cyclohexanone-3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:ethyl 2-O-4-(2-(dimethylsilyloxy)ethyl)cyclohexanone-3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside
CAS No.:1180492-33-4
Molecular Formula:C₃₉H₅₂O₇SSi
Molecular Weight:692.989
Hs Code.:

Synonyms:ethyl 2-O-4-(2-(dimethylsilyloxy)ethyl)cyclohexanone-3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

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Chemical Property of ethyl 2-O-4-(2-(dimethylsilyloxy)ethyl)cyclohexanone-3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

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Technology Process of ethyl 2-O-4-(2-(dimethylsilyloxy)ethyl)cyclohexanone-3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

There total 1 articles about ethyl 2-O-4-(2-(dimethylsilyloxy)ethyl)cyclohexanone-3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 32863-01-7
4-(2-hydroxyethyl)cyclohexan-1-one

: 1180492-09-4
ethyl 2-O-dimethylsilane-3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

: 1180492-33-4
ethyl 2-O-4-(2-(dimethylsilyloxy)ethyl)cyclohexanone-3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

: C₇₀H₉₂O₁₂S₂Si₂

Guidance literature:: With potassium tert-butylate; 1,3-bis(mesityl)imidazolium chloride; copper(l) chloride; In toluene; at 20 ℃; for 3h; Inert atmosphere;

Reference yield: 62.0%

: 1180492-33-4
ethyl 2-O-4-(2-(dimethylsilyloxy)ethyl)cyclohexanone-3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

: 1180492-35-6
ethyl 2-O-4-(2-(dimethylsilyloxy)ethyl)cyclohexanone-3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

Guidance literature:: ethyl 2-O-4-(2-(dimethylsilyloxy)ethyl)cyclohexanone-3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside; With N-iodo-succinimide; 2,6-di-tert-butyl-4-methylpyridine; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -40 - 0 ℃; Inert atmosphere;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane; at 0 - 20 ℃; Inert atmosphere;