1D-O-(1,2-di-O-palmitoyl-sn-glycerol-3-O-methylphospho)-2,3,5,6-O-tetrakis(methoxymethylene)-myo-inositol-4-(dibenzyl phosphate)

Base Information

Chemical Name:1D-O-(1,2-di-O-palmitoyl-sn-glycerol-3-O-methylphospho)-2,3,5,6-O-tetrakis(methoxymethylene)-myo-inositol-4-(dibenzyl phosphate)
CAS No.:496808-64-1
Molecular Formula:C₆₄H₁₁₀O₂₀P₂
Molecular Weight:1261.51
Hs Code.:

Synonyms:1D-O-(1,2-di-O-palmitoyl-sn-glycerol-3-O-methylphospho)-2,3,5,6-O-tetrakis(methoxymethylene)-myo-inositol-4-(dibenzyl phosphate)

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Chemical Property of 1D-O-(1,2-di-O-palmitoyl-sn-glycerol-3-O-methylphospho)-2,3,5,6-O-tetrakis(methoxymethylene)-myo-inositol-4-(dibenzyl phosphate)

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Technology Process of 1D-O-(1,2-di-O-palmitoyl-sn-glycerol-3-O-methylphospho)-2,3,5,6-O-tetrakis(methoxymethylene)-myo-inositol-4-(dibenzyl phosphate)

There total 10 articles about 1D-O-(1,2-di-O-palmitoyl-sn-glycerol-3-O-methylphospho)-2,3,5,6-O-tetrakis(methoxymethylene)-myo-inositol-4-(dibenzyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 496808-59-4
Hexadecanoic acid (R)-2-(diisopropylamino-methoxy-phosphanyloxy)-1-hexadecanoyloxymethyl-ethyl ester

: 496808-63-0
1D-2,3,5,6-O-tetrakis(methoxymethylene)-myo-inositol-4-(dibenzyl phosphate)

: 496808-64-1
1D-O-(1,2-di-O-palmitoyl-sn-glycerol-3-O-methylphospho)-2,3,5,6-O-tetrakis(methoxymethylene)-myo-inositol-4-(dibenzyl phosphate)

Guidance literature:: Hexadecanoic acid (R)-2-(diisopropylamino-methoxy-phosphanyloxy)-1-hexadecanoyloxymethyl-ethyl ester; 1D-2,3,5,6-O-tetrakis(methoxymethylene)-myo-inositol-4-(dibenzyl phosphate); With 1H-tetrazole; In acetonitrile; at 20 ℃; for 24h;

With 3-chloro-benzenecarboperoxoic acid; In chloroform; acetonitrile; at -30 ℃; Further stages.;
DOI:10.1021/jo0206418

Reference yield:

: 108549-23-1
Dibenzyl N,N-diisopropylphosphoramidite

: 496808-64-1
1D-O-(1,2-di-O-palmitoyl-sn-glycerol-3-O-methylphospho)-2,3,5,6-O-tetrakis(methoxymethylene)-myo-inositol-4-(dibenzyl phosphate)

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrazole

2.1: 3-chloroperoxybenzoic acid / -30 °C

3.1: tetra-n-butylammonium fluoride / tetrahydrofuran / 1 h

4.1: tetrazole / acetonitrile / 24 h / 20 °C

4.2: 95 percent / 3-chloropreoxybenzoic acid / acetonitrile; CHCl₃ / -30 °C

With 1H-tetrazole; tetrabutyl ammonium fluoride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo0206418

Reference yield:

: 331679-26-6
2,3-O-(D-1,7,7-trimethylbicyclo[2.2.1]hept-6-ylidene)-D-myo-inositol

: 496808-64-1
1D-O-(1,2-di-O-palmitoyl-sn-glycerol-3-O-methylphospho)-2,3,5,6-O-tetrakis(methoxymethylene)-myo-inositol-4-(dibenzyl phosphate)

Guidance literature:: Multi-step reaction with 9 steps

1.1: 88 percent / imidazole

2.1: 90 percent / HSCH₂CH₂OH; BF₃*Et₂O

3.1: pyridine

3.2: trifluoroacetic acid / H₂O; CHCl₃

4.1: 90 percent / diisopropylethylamine / dimethylformamide / 24 h / 65 °C

5.1: 86 percent / sodium methoxide / methanol / 3 h

6.1: tetrazole

7.1: 3-chloroperoxybenzoic acid / -30 °C

8.1: tetra-n-butylammonium fluoride / tetrahydrofuran / 1 h

9.1: tetrazole / acetonitrile / 24 h / 20 °C

9.2: 95 percent / 3-chloropreoxybenzoic acid / acetonitrile; CHCl₃ / -30 °C

With pyridine; 1H-imidazole; 1H-tetrazole; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; sodium methylate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; 2-hydroxyethanethiol; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo0206418