Technology Process of C14H16O3Se
There total 6 articles about C14H16O3Se which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
benzene;
at 20 ℃;
for 0.5h;
Inert atmosphere;
Irradiation;
DOI:10.1021/ol201758a
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: (1S)-10-camphorsulfonic acid / benzene / 4 h / 20 °C
2.1: ozone / dichloromethane / 0.5 h / -78 °C
2.2: -78 - 20 °C
2.3: 0 - 20 °C
3.1: oxalyl dichloride / benzene / 3 h / 20 °C
3.2: 1 h / 20 °C / Darkness
4.1: benzene / 0.5 h / 20 °C / Inert atmosphere; Irradiation
With
oxalyl dichloride; (1S)-10-camphorsulfonic acid; ozone;
In
dichloromethane; benzene;
DOI:10.1021/ol201758a
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: Dowex-50W-4 / methanol / 20 h / 20 °C
2.1: (1S)-10-camphorsulfonic acid / benzene / 4 h / 20 °C
3.1: ozone / dichloromethane / 0.5 h / -78 °C
3.2: -78 - 20 °C
3.3: 0 - 20 °C
4.1: oxalyl dichloride / benzene / 3 h / 20 °C
4.2: 1 h / 20 °C / Darkness
5.1: benzene / 0.5 h / 20 °C / Inert atmosphere; Irradiation
With
oxalyl dichloride; (1S)-10-camphorsulfonic acid; ozone;
In
methanol; dichloromethane; benzene;
DOI:10.1021/ol201758a