(2,6-(2,4,6-Me₃C₆H₂)2C₆H₃)(2-(2,4,6-Me₃C₆H₂)C₆H₄)N₃H

Base Information

Chemical Name:(2,6-(2,4,6-Me₃C₆H₂)2C₆H₃)(2-(2,4,6-Me₃C₆H₂)C₆H₄)N₃H
CAS No.:869383-21-1
Molecular Formula:C₃₉H₄₁N₃
Molecular Weight:551.775
Hs Code.:

(2,6-(2,4,6-Me<sub>3</sub>C<sub>6</sub>H<sub>2</sub>)2C<sub>6</sub>H<sub>3</sub>)(2-(2,4,6-Me<sub>3</sub>C<sub>6</sub>H<sub>2</sub>)C<sub>6</sub>H<sub>4</sub>)N<sub>3</sub>H

Synonyms:(2,6-(2,4,6-Me₃C₆H₂)2C₆H₃)(2-(2,4,6-Me₃C₆H₂)C₆H₄)N₃H

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Chemical Property of (2,6-(2,4,6-Me₃C₆H₂)2C₆H₃)(2-(2,4,6-Me₃C₆H₂)C₆H₄)N₃H

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Technology Process of (2,6-(2,4,6-Me₃C₆H₂)2C₆H₃)(2-(2,4,6-Me₃C₆H₂)C₆H₄)N₃H

There total 1 articles about (2,6-(2,4,6-Me₃C₆H₂)2C₆H₃)(2-(2,4,6-Me₃C₆H₂)C₆H₄)N₃H which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 477933-79-2
2'-azido-2,4,6,2'',4'',6''-hexamethyl-[1,1';3',1'']terphenyl

: 1-iodo-2-(2′,4′,6′-trimethylphenyl)benzene

: 869383-21-1
(2,6-(2,4,6-Me₃C₆H₂)2C₆H₃)(2-(2,4,6-Me₃C₆H₂)C₆H₄)N₃H

Guidance literature:: 1-iodo-2-(2′,4′,6′-trimethylphenyl)benzene; With n-butyllithium; In diethyl ether; hexane; cooling;

2'-azido-2,4,6,2'',4'',6''-hexamethyl-[1,1';3',1'']terphenyl; In diethyl ether; hexane;
DOI:10.1002/anie.200501494

Reference yield: 72.0%

: 869383-21-1
(2,6-(2,4,6-Me₃C₆H₂)2C₆H₃)(2-(2,4,6-Me₃C₆H₂)C₆H₄)N₃H

: 20398-06-5
thallium (I) ethoxide

: TlN₃(2,6-(2,4,6-Me₃C₆H₂)2C₆H₃)(2-(2,4,6-Me₃C₆H₂)C₆H₄)

Guidance literature:: In n-heptane; toluene; under Ar atm. TlOEt was added at 0°C to soln. ligand in n-heptane- toluene (4:1), stirred for 30 min, and heated to 80°C; afrer centrifugation soln. was kept overnight at room temp.; elem. anal.;
DOI:10.1021/ic800029z

Reference yield: 59.0%

: 869383-21-1
(2,6-(2,4,6-Me₃C₆H₂)2C₆H₃)(2-(2,4,6-Me₃C₆H₂)C₆H₄)N₃H

: mercury dibromide

: 1241550-60-6,1241550-61-7
bromo-[[[N'-2-(2',4',6'-trimethyl)biphenyl]-(N'''-2,4,6,2'',4'',6''-hexamethyl-1,1':3',1''-terphen-2'-yl)]triazenido-N']mercury

Guidance literature:: With nBuLi; In diethyl ether; hexane; byproducts: LiBr, nBuH; under Ar, using Schlenk technique; to stirred cooled soln. of triazene deriv. in ethyl ether added n-BuLi in hexane; stirred for 30 min; HgCl2 added, stirred at ambient temp. for 4 h; volatile materials removed under reduced pressure; solid extd. with n-heptane; LiBr separated by centrifugation, filtrate concd., cooled at -20°C;
DOI:10.1002/zaac.200900482