(E)-1-dodecylsulfanyl-2-phenylethenyl diphenyldithiophosphinate

Base Information

Chemical Name:(E)-1-dodecylsulfanyl-2-phenylethenyl diphenyldithiophosphinate
CAS No.:1034014-66-8
Molecular Formula:C₃₂H₄₁PS₃
Molecular Weight:552.849
Hs Code.:

Synonyms:(E)-1-dodecylsulfanyl-2-phenylethenyl diphenyldithiophosphinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-dodecylsulfanyl-2-phenylethenyl diphenyldithiophosphinate

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Technology Process of (E)-1-dodecylsulfanyl-2-phenylethenyl diphenyldithiophosphinate

There total 1 articles about (E)-1-dodecylsulfanyl-2-phenylethenyl diphenyldithiophosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1034014-59-9
1-(dodec-1-ylsulfanyl)-2-phenylethyne

: 1015-38-9
diphenylphosphinodithioic acid

: 1034014-66-8
(E)-1-dodecylsulfanyl-2-phenylethenyl diphenyldithiophosphinate

Guidance literature:: In ethanol; at 25 ℃; for 5h; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1246/bcsj.81.506

Reference yield: 85.0%

: 1034014-66-8
(E)-1-dodecylsulfanyl-2-phenylethenyl diphenyldithiophosphinate

: 1034014-58-8
dodecyl phenylethanedithioate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 25 ℃; for 4h; Inert atmosphere;
DOI:10.1246/bcsj.81.506

Reference yield: 67.0%

: 109-72-8,29786-93-4
n-butyllithium

: 1034014-66-8
(E)-1-dodecylsulfanyl-2-phenylethenyl diphenyldithiophosphinate

: 1-butylsulfanyl-2-phenylethenyl dodecyl sulfide

Guidance literature:: n-butyllithium; (E)-1-dodecylsulfanyl-2-phenylethenyl diphenyldithiophosphinate; In tetrahydrofuran; hexane; cyclohexane; at 0 ℃; for 0.5h; Inert atmosphere;

With water; In tetrahydrofuran; hexane; cyclohexane;

With silica gel;
DOI:10.1246/bcsj.81.506